hydrogenchloride; water in acetonitrile T=20°C; 12 h;
参考文献
He, Zhi; Zajdlik, Adam; St. Denis, Jeffrey D.; Assem, Naila; Yudin, Andrei K.
Journal of the American Chemical Society, 2012 , vol. 134, # 24 p. 9926 - 9929
hydrogenchloride; water in acetonitrile T=23°C; 48 h;
参考文献
He, Zhi; Zajdlik, Adam; St. Denis, Jeffrey D.; Assem, Naila; Yudin, Andrei K.
Journal of the American Chemical Society, 2012 , vol. 134, # 24 p. 9926 - 9929
1: tetrakis(triphenylphosphine) palladium(0); triethyl borane; triethylamine / tetrahydrofuran / Molecular sieve 2: sodium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol; cyclohexene / 12 h / 20 °C 3: diphenyl phosphoryl azide; triethylamine / acetonitrile / 2 h / 50 °C / Inert atmosphere 4: hydrogenchloride; water / acetonitrile / 48 h / 23 °C View Scheme
参考文献
He, Zhi; Zajdlik, Adam; St. Denis, Jeffrey D.; Assem, Naila; Yudin, Andrei K.
Journal of the American Chemical Society, 2012 , vol. 134, # 24 p. 9926 - 9929
1: sodium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol; cyclohexene / 20 °C 2: diphenyl phosphoryl azide; triethylamine / acetonitrile / 1 h / 50 °C / Inert atmosphere 3: hydrogenchloride; water / acetonitrile / 12 h / 20 °C View Scheme
参考文献
He, Zhi; Zajdlik, Adam; St. Denis, Jeffrey D.; Assem, Naila; Yudin, Andrei K.
Journal of the American Chemical Society, 2012 , vol. 134, # 24 p. 9926 - 9929
1: diphenyl phosphoryl azide; triethylamine / acetonitrile / 1 h / 50 °C / Inert atmosphere 2: hydrogenchloride; water / acetonitrile / 12 h / 20 °C View Scheme
参考文献
He, Zhi; Zajdlik, Adam; St. Denis, Jeffrey D.; Assem, Naila; Yudin, Andrei K.
Journal of the American Chemical Society, 2012 , vol. 134, # 24 p. 9926 - 9929
1: sodium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol; cyclohexene / 12 h / 20 °C 2: diphenyl phosphoryl azide; triethylamine / acetonitrile / 2 h / 50 °C / Inert atmosphere 3: hydrogenchloride; water / acetonitrile / 48 h / 23 °C View Scheme
参考文献
He, Zhi; Zajdlik, Adam; St. Denis, Jeffrey D.; Assem, Naila; Yudin, Andrei K.
Journal of the American Chemical Society, 2012 , vol. 134, # 24 p. 9926 - 9929
1: diphenyl phosphoryl azide; triethylamine / acetonitrile / 2 h / 50 °C / Inert atmosphere 2: hydrogenchloride; water / acetonitrile / 48 h / 23 °C View Scheme
参考文献
He, Zhi; Zajdlik, Adam; St. Denis, Jeffrey D.; Assem, Naila; Yudin, Andrei K.
Journal of the American Chemical Society, 2012 , vol. 134, # 24 p. 9926 - 9929
