反应条件
1: 83 percent / Na2CO3 / H2O / a) 70 deg C, 1 h, b) r.t., 13 h
2: 62 percent / 30percent H2O2, AcOH / 10 h / 23 °C
3: 89 percent / SOCl2, pyridine / CH2Cl2 / a) 0 deg C, 15 min, b) 40 deg C, 5 min
4: 97 percent / NEt3 / toluene / 15 h / 25 °C
View Scheme
参考文献
Leblanc, Andre; Fosset, Laurent; Magnaud, Gilbert; Delmas, Gerard; Desgranges, Michel; et al.
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 79, # 1,4 p. 141 - 146
