反应条件
tetraoctylammonium bromide; NaBH4 in tetrahydrofuran; water
tetraoctylammonium bromide and Au complex dissolved in THF, cooled to 0°C over 30 min; HSCH2CH2Ph added slowly; aq. NaBH4 added rapidly under stirring; reacted with stirring for 4 h; water layer removed; cold water added; ppt. collected; washed with waterand MeOH, dried under reduced pressure at room temp.; recrystd. twice f rom CH3CN/MeOH and toluene/CH3OH;
参考文献
Wu, Zhikun
Angewandte Chemie - International Edition, 2012 , vol. 51, # 12 p. 2934 - 2938
