4-(4-羟基-偶氮苯)苯甲酸乙酯合成路线 （共 5 条）
反应条件
1: potassium carbonate / pentan-3-one / Reflux 2: sodium hydroxide View Scheme
参考文献
Morita, Yuki; Uemura, Hiroshi; Shimoi, Kentaro; Kasatani, Kazuo; Okamoto, Hiroaki
Molecular Crystals and Liquid Crystals, 2009 , vol. 508, p. 163 - 172
反应条件
1.1: potassium iodide; potassium carbonate / butanone / 6 h / |Reflux
2.1: potassium hydroxide / ethanol / 12 h / |Reflux
2.2: 20 °C
View Scheme
参考文献
Alaasar, Mohammed; Prehm, Marko; May, Kathrin; Eremin, Alexey; Tschierske, Carsten
Advanced Functional Materials, 2014 , vol. 24, # 12 p. 1703 - 1717
反应条件
1: 98 percent / K2CO3 / acetone / 10 h / Heating
2: 99 percent / NaOH; water / methanol / 6 h / Heating
View Scheme
参考文献
Morita, Yuki; Uemura, Hiroshi; Shimoi, Kentaro; Kasatani, Kazuo; Okamoto, Hiroaki
Molecular Crystals and Liquid Crystals, 2009 , vol. 508, p. 163 - 172
反应条件
1: 87 percent / K2CO3 / acetone / 10 h / Heating
2: 76 percent / NaOH; water / methanol / 6 h / Heating
View Scheme
参考文献
Alaasar, Mohammed; Prehm, Marko; May, Kathrin; Eremin, Alexey; Tschierske, Carsten
Advanced Functional Materials, 2014 , vol. 24, # 12 p. 1703 - 1717
反应条件
Multi-step reaction with 2 steps 1: hydrogenchloride; sodium nitrite / water2: sulfuric acid / Reflux
参考文献
Morita, Yuki; Uemura, Hiroshi; Shimoi, Kentaro; Kasatani, Kazuo; Okamoto, Hiroaki Molecular Crystals and Liquid Crystals, 2009 , vol. 508, p. 163 - 172
