4-羟基-3-甲氧基苯甲腈合成路线 （共 46 条）
反应条件
anhydrous iron chloride; hydroxylamine hydrochloride in N,N-dimethyl-formamide 3 h; Reflux; Reagent/catalyst;
参考文献
Ghosh, Pranab; Subba, Raju
Tetrahedron Letters, 2013 , vol. 54, # 36 p. 4885 - 4887
反应条件
caesium carbonate in N,N-dimethyl-formamide T=130°C; 10 h; Schlenk technique;
参考文献
Sajadi, S. Mohammad; Maham, Mehdi; Mahmoud, Sarbast Ahmad
Journal of Chemical Research, 2013 , vol. 37, # 10 p. 620 - 622
反应条件
silica gel 0.0166667 h; microwave irradiation;
参考文献
Jie, Zhou; Rammoorty, Vebumani; Fischer, Bilha
Journal of Organic Chemistry, 2002 , vol. 67, # 3 p. 711 - 719
反应条件
sodium hydroxide; ammonia in water
反应条件
1,3-dimethyl-imidazolidin-2-one; sodium hexamethyldisilazane in tetrahydrofuran T=185°C; 12 h; further reagent: LDA;
参考文献
Journal of Organic Chemistry, , vol. 62, # 12 p. 4097 - 4104
反应条件
sodium hexamethyldisilazane in tetrahydrofuran T=110°C; 24 h;
参考文献
Synthesis, , # 3 p. 329 - 332
反应条件
tetrabutylammomium bromide; copper (II) acetate monohydrate in water T=180°C; 22 h;
参考文献
Ren, Yunlai; Zhao, Shuang; Tian, Xinzhe; Liu, Zhifei; Wang, Jianji; Yin, Weiping
Letters in Organic Chemistry, 2009 , vol. 6, # 7 p. 564 - 567
反应条件
1: With triethylamine in N,N-dimethyl-formamide; toluene Curtius rearrangement; 3 h; Heating; 2: With potassium hydroxide; glycerol in ethanol; N,N-dimethyl-formamide; toluene 2 h; Heating; Further stages.;
参考文献
Spurg, Anke; Waldvogel, Siegfried R.
European Journal of Organic Chemistry, 2008 , # 2 p. 337 - 342
参考文献
Chemische Berichte, , vol. 24, p. 3652
反应条件
sodium hexamethyldisilazane in tetrahydrofuran T=185°C; 24 h;
参考文献
Synthesis, , # 3 p. 329 - 332
