3-(4-甲基苯基)吡啶合成路线 （共 66 条）
反应条件
1: 1.) 1 M aq. HCl, NaNO2 / 1.) 0 deg C, 30 min, 2.) 0 deg C, 30 min
2: CF3COOH / 3 h / 65 - 70 °C
View Scheme
参考文献
Patrick, Timothy B.; Willaredt, Richard P.; DeGonia, David J.
Journal of Organic Chemistry, 1985 , vol. 50, # 13 p. 2232 - 2235
反应条件
1,10-phenanthroline; palladium diacetate; caesium carbonate
T=140°C; 48 h; Sealed tube;
参考文献
Ye, Mengchun; Gao, Guo-Lin; Edmunds, Andrew J. F.; Worthington; Morris, James A.; Yu, Jin-Quan
Journal of the American Chemical Society, 2011 , vol. 133, # 47 p. 19090 - 19093
反应条件
Br(1-)*C18H28N3(1+); sodium t-butanolate
T=110°C; 4 h; Inert atmosphere;
参考文献
Chen, Wen-Ching; Hsu, Yu-Chen; Shih, Wei-Chun; Lee, Ching-Yu; Chuang, Wen-Han; Tsai, Yi-Fang; Chen, Peter Ping-Yu; Ong, Tiow-Gan
Chemical Communications, 2012 , vol. 48, # 53 p. 6702 - 6704
反应条件
T=20°C; 24 h; Sealed tube; Overall yield = 53 percent;
参考文献
Li, Yahui; Liu, Wei; Kuang, Chunxiang
Chemical Communications, 2014 , vol. 50, # 54 p. 7124 - 7127
反应条件
1 h; Ambient temperatureIrradiation; Title compound not separated from byproducts;
参考文献
Ohkura, Kazue; Seki, Koh-ichi; Terashima, Masanao; Kanaoka, Yuichi
Tetrahedron Letters, 1989 , vol. 30, # 26 p. 3433 - 3436
反应条件
200 h; Ambient temperatureIrradiationisotope effects; other p-tolyl radical sources;
参考文献
Nakabayashi, Takeshige; Horii, Toyokazu; Kawamura, Shunichi; Abe, Yasuo
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 8 p. 2535 - 2536
