4-甲基-2-(1-甲乙基)苯酚合成路线 (共 27 条)
反应条件
potassium hydroxide; hydrazine hydrate in diethylene glycol T=210°C; 1 h;
参考文献
Martin, Robert; Demerseman, Pierre
Monatshefte fuer Chemie, 1990 , vol. 121, p. 227 - 236
反应条件
boron trifluoride T=85°C;
参考文献
Smith
Journal of the American Chemical Society, 1934 , vol. 56, p. 717,718
Journal of the American Chemical Society, 1937 , vol. 59, p. 899
反应条件
sulfated zirconia T=180°C; 2 h;
参考文献
Yadav, Ganapati D.; Pathre, Ganesh S.
Synthetic Communications, 2008 , vol. 38, # 15 p. 2684 - 2691
反应条件
Fuller's Earth; sulfuric acid T=180°C;
参考文献
Carpenter; Easter
Journal of Organic Chemistry, 1955 , vol. 20, p. 401,407
参考文献
Schering-Kahlbaum A.G.
Patent: GB273685 , 1927 ;
反应条件
montmorillonite clay; sulfuric acid T=180°C; 3 h;
参考文献
McPhail, Kerry L.; Rivett, Douglas E.A.; Lack, David E.; Davies-Coleman, Michael T.
Tetrahedron, 2000 , vol. 56, # 47 p. 9391 - 9396
反应条件
1: 72 percent / TiCl4 / CH2Cl2 / 4 h / -5 - 0 °C 2: 82 percent / N2H4*H2O, KOH / bis-(2-hydroxy-ethyl) ether / 1 h / 210 °C View Scheme
参考文献
Martin, Robert; Demerseman, Pierre
Monatshefte fuer Chemie, 1990 , vol. 121, p. 227 - 236
反应条件
10 palladium on active carbon in acetic acid
参考文献
Dinge, A. S.; Kirtany, J. K.; Paknikar, S. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 3 p. 245 - 246
反应条件
2: Pd-C(10percent) / acetic acid View Scheme
参考文献
Dinge, A. S.; Kirtany, J. K.; Paknikar, S. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 3 p. 245 - 246
反应条件
T=250 - 350°C; Leiten ueber Thoriumoxyd, Aluminiumoxyd oder Aluminiumphosphat;
参考文献
Rhein. Kampfer-Fabr.
Patent: DE586150 , 1927 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 19, p. 709
Full Text Show Details
Carpenter; Easter
Journal of Organic Chemistry, 1955 , vol. 20, p. 401,407