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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5-氟靛红
合成路线
（共 52 条）
879274-72-3
→
反应条件
443-69-6
5-氟靛红
反应条件
sulfuric acid in water T=50 - 90°C;
参考文献
Wilson, Dean; Fanning, Lev T.D.; Krenitsky, Paul; Termin, Andreas; Joshi, Pramod; Sheth, Urvi
Patent: US2008/167305 A1, 2008 ;
Location in patent: Page/Page column 40 ;
515-83-3
2,2,2-三氯-1-乙氧基乙醇
+
371-40-4
4-氟苯胺
→
反应条件
443-69-6
5-氟靛红
反应条件
1: With hydrogenchloride; sodium sulfate in water 1 h; 2: With hydroxylamine hydrochloride in water T=10 - 80°C; 1.5 h; 3: With sulfuric acid T=60°C; 6 h;
参考文献
Xie, Wenge; Herbert, Brian; Ma, Jianguo; Nguyen, Truc Minh; Schumacher, Richard; Gauss, Carla Maria; Tehim, Ashok
Patent: US2005/250808 A1, 2005 ;
Location in patent: Page/Page column 39 ;
US 20050250808 A1
351-09-7
4-氟异硝基联苯胺
→
反应条件
443-69-6
5-氟靛红
反应条件
sulfuric acid Cyclization; 0.0111111 h; microwave irradiation;
参考文献
Jnaneshwara; Bedekar; Deshpande
Synthetic Communications, 1999 , vol. 29, # 20 p. 3627 - 3633
201230-82-2
→
反应条件
443-69-6
5-氟靛红
反应条件
1: N'-(2-bromo-4-fluorophenyl)-N,N-dimethylurea With methyllithium in tetrahydrofuran; diethyl ether T=0°C; 2: With tert.-butyl lithium in tetrahydrofuran; diethyl ether; n-heptane T=0°C; 1 h; 3: carbon monoxide in tetrahydrofuran; diethyl ether; n-heptane T=0°C; 0.5 h;
参考文献
Smith, Keith; El-Hiti, Gamal A.; Hawes, Anthony C.
Synthesis, 2003 , # 13 p. 2047 - 2052
20780-76-1
5-碘吲哚醌
→
反应条件
443-69-6
5-氟靛红
反应条件
1: With tetrakis(triphenylphosphine) palladium(0); 1,1,1,2,2,2-hexabutyl-distannane; lithium chloride in 1,4-dioxane T=23 - 100°C; Inert atmosphere; 2: With silver trifluoromethanesulfonate; F-TEDA-PF6 in acetone T=23°C; 0.333333 h; Inert atmosphere; regiospecific reaction;
参考文献
Furuya, Takeru; Strom, Alexandra E.; Ritter, Tobias
Journal of the American Chemical Society, 2009 , vol. 131, p. 1662 - 1663
1174558-44-1
→
反应条件
443-69-6
5-氟靛红
反应条件
hydrogenchloride; acetic acid in water 0.333333 h; Reflux;
参考文献
Huber, Stefan M.; Hennig, Andre; Puehlhofer, Frank G.; Weiss, Robert
Journal of Heterocyclic Chemistry, 2009 , vol. 46, # 3 p. 421 - 427
79-37-8
草酰氯
+
371-40-4
4-氟苯胺
→
反应条件
443-69-6
5-氟靛红
反应条件
H-β zeolite in 1,2-dichloro-ethane T=80°C; 36 h; Inert atmosphere;
参考文献
Victor Paul Raj; Shaikh, Tanveer Mahamadali; Sudalai, Arumugam
Acta Chimica Slovenica, 2010 , vol. 57, # 2 p. 466 - 469
302-17-0
水合氯醛
+
371-40-4
4-氟苯胺
→
反应条件
443-69-6
5-氟靛红
反应条件
1: With hydrogenchloride; hydroxylamine hydrochloride; sodium sulfate 0.166667 h; Heating; 2: With sulfuric acid 1 h; Heating;
参考文献
Chouhan, Mangilal; Senwar, Kishna Ram; Sharma, Ratnesh; Grover, Vikas; Nair, Vipin A.
Green Chemistry, 2011 , vol. 13, # 9 p. 2553 - 2560
371-40-4
4-氟苯胺
→
反应条件
443-69-6
5-氟靛红
反应条件
1: hydroxylamine sulfate; sodium sulfate; HCl / ethanol; H2O 2: H2SO4 View Scheme
参考文献
Joshi; Patni; Chand; Sharma; Bhattacharya; Rao
Pharmazie, 1984 , vol. 39, # 3 p. 153 - 155
113423-50-0
→
反应条件
443-69-6
5-氟靛红
反应条件
water in methanol 2 h; Heating;
参考文献
Rossiter, Sharon
Tetrahedron Letters, 2002 , vol. 43, # 26 p. 4671 - 4673
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