in tetrahydrofuran under N2; soln. of 5mmol NaMn(CO)5 in THF cooled to -78°C, 5.25 mmol (PhO)2CHCl added; mixt. warmed up to room temp., then stirred for 3 h; pptd. NaCl filtered off, solvent removed; residue extd. with pentane; pentane soln. cooled, ppt. recrystd. from pentane;
Livantsov, M. V.; Proskurnina, M. V.; Prishchenko, A. A.; Lutsenko, I. F.
J. Gen. Chem. USSR (Engl. Transl.), 1984 , vol. 54, # 11 p. 2504 - 2517,2237 - 2249