N-苄氧羰基-DL-蛋氨酸合成路线 (共 17 条)
反应条件
sodium hydrogencarbonate T=23°C; 24 h;
参考文献
Rosenthal, Gerald A.; Dahlman, D. L.; Crooks, Peter A.; Phuket, Supinan Na; Trifonov, L. S.
Journal of Agricultural and Food Chemistry, 1995 , vol. 43, # 10 p. 2728 - 2734
反应条件
industrial papain T=50°C; 4 h; pH 4,5 (citrate buffer, cystein*HCl);
参考文献
Moriniere, J. L.; Danree, B.; Lemoine, J.; Guy, A.
Synthetic Communications, 1988 , vol. 18, # 4 p. 441 - 444
反应条件
D,L-Cysteine; papain T=38°C; gepufferte wss. Loesung (pH 5);
参考文献
Dekker; Fruton
Journal of Biological Chemistry, 1948 , vol. 173, p. 471,475, 476
反应条件
1: aqueous NaOH / 0 °C 2: unter Zusatz von Papain und Cystein in gepufferter wss.Loesung <pH 5> View Scheme
参考文献
Dekker; Fruton
Journal of Biological Chemistry, 1948 , vol. 173, p. 471,475, 476
反应条件
resolved on CSP cellulose tris(3,5-dimethylphenylcarbamate) by chiral HPLC;
参考文献
Okamoto, Yoshio; Aburatani, Ryo; Kaida, Yuriko; Hatada, Koichi
Chemistry Letters, 1988 , p. 1125 - 1128
反应条件
T=38°C; gepufferte wss. Loesung (pH 5);
参考文献
Dekker; Fruton
Journal of Biological Chemistry, 1948 , vol. 173, p. 471,475, 476
反应条件
1: unter Zusatz von Papain und Cystein in gepufferter wss.Loesung <pH 5> 2: palladium; glacial acetic acid; methanol / durch Hydrogenolyse View Scheme
参考文献
Dekker; Fruton
Journal of Biological Chemistry, 1948 , vol. 173, p. 471,475, 476
反应条件
industrial papain T=50°C; 4 h; pH 4,5 (citrate buffer, cystein*HCl);
参考文献
Moriniere, J. L.; Danree, B.; Lemoine, J.; Guy, A.
Synthetic Communications, 1988 , vol. 18, # 4 p. 441 - 444
反应条件
D,L-Cysteine; papain T=38°C; gepufferte wss. Loesung (pH 5);
参考文献
Dekker; Fruton
Journal of Biological Chemistry, 1948 , vol. 173, p. 471,475, 476
反应条件
resolved on CSP cellulose tris(3,5-dimethylphenylcarbamate) by chiral HPLC;
参考文献
Okamoto, Yoshio; Aburatani, Ryo; Kaida, Yuriko; Hatada, Koichi
Chemistry Letters, 1988 , p. 1125 - 1128