1-碘-2,4,6-三硝基苯合成路线 (共 13 条)
反应条件
phosphorus pentoxide; N,N-dimethyl-formamide; zinc(II) iodide
T=60 - 70°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Zbarskii, V. L.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 11.2 p. 2185 - 2186
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 11 p. 2460 - 2461
反应条件
potassium trimethylstannate in tetrahydrofuran
T=0 - 5°C;
参考文献
Artamkina, G. A.; Egorov, M. P.; Kharitonov, V. G.; Beletskaya, I. P.; Reutov, O. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 3 p. 640
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 3 p. 715 - 716
反应条件
in tetrahydrofuran
72 h; Yields of byproduct given;
参考文献
Artamkina, G. A.; Egorov, M. P.; Beletskaya, I. P.; Reutov, O. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , p. 1649 - 1659
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 8 p. 1809 - 1820