2-(4-吗啉基甲基)苯酚合成路线 (共 11 条)
参考文献
Fields,D.L. et al.
Journal of Organic Chemistry, 1964 , vol. 29, p. 2640 - 2647
反应条件
water in various solvent(s) T=99°C; hydrolysis rate constants at pH 8.83 and 10.0; Rate constant;
参考文献
Teitel'baum, A. B.; Kudryavtseva, L. A.; Bel'skii, V. E.; Ivanov, V. E.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 1 p. 72 - 75
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 1 p. 81 - 85
反应条件
in benzene
Condensation; Mannich reaction; 6 h; Heating;
参考文献
Tian, Jing-Zhi; Zhang, Jin-Qi; Shen, Xi; Zou, Hui-Xian
Journal of Organometallic Chemistry, 1999 , vol. 584, # 2 p. 240 - 245
反应条件
sodium hydroxide
T=80°C; pH=12; 1 h;
参考文献
Modica; Zanaletti; Freccero; Mella
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 41 - 52
反应条件
nido-decaborane in methanol
T=20°C; Reductive amination; 1 h;
参考文献
Bae, Jong Woo; Lee, Seung Hwan; Cho, Young Jin; Yoon, Cheol Min
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 2 p. 145 - 146
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=0 - 20°C;
参考文献
Assimomytis, Nikos; Sariyannis, Yiannis; Stavropoulos, Georgios; Tsoungas, Petros G.; Varvounis, George; Cordopatis, Paul
Synlett, 2009 , # 17 p. 2777 - 2782
反应条件
sodium isopropanolate in isopropyl alcohol
40 h; Heating;
参考文献
Katritzky, Alan R.; Zhang, Zhongxing; Lan, Xiangfu; Lang, Hengyaun
Journal of Organic Chemistry, 1994 , vol. 59, # 7 p. 1900 - 1903
反应条件
bis(acetylacetonate)oxovanadium in dichloromethane
48 h; Heating;
参考文献
Hwang, Der-Ren; Uang, Biing-Jiun
Organic Letters, 2002 , vol. 4, # 3 p. 463 - 466
反应条件
T=20°C; Mannich reaction; P=6000600 Torr; 72 h; regioselective reaction;
参考文献
Matsumoto, Kiyoshi; Joho, Kouta; Mimori, Seisuke; Iida, Hirokazu; Hamana, Hiroshi; Kakehi, Akikazu
Heterocycles, 2008 , vol. 76, # 2 p. 1061 - 1067
反应条件
sodium carbonate in water
pH=9.0; Kinetics;
参考文献
Weinert, Emily E.; Dondi, Ruggero; Colloredo-Melz, Stefano; Frankenfield, Kristen N.; Mitchell, Charles H.; Freccero, Mauro; Rokita, Steven E.
Journal of the American Chemical Society, 2006 , vol. 128, # 36 p. 11940 - 11947