boron tribromide in dichloromethane T=-78 - 20°C; 16 h;
参考文献
Dumez, Estelle; Snaith, John S.; Jackson, Richard F. W.; McElroy, Andrew B.; Overington, John; Wythes, Martin J.; Withka, Jane M.; McLellan, Thomas J.
Journal of Organic Chemistry, 2002 , vol. 67, # 14 p. 4882 - 4892
Dumez, Estelle; Snaith, John S.; Jackson, Richard F. W.; McElroy, Andrew B.; Overington, John; Wythes, Martin J.; Withka, Jane M.; McLellan, Thomas J.
Journal of Organic Chemistry, 2002 , vol. 67, # 14 p. 4882 - 4892
1.1: t-BuLi / diethyl ether; pentane / 22 h / -25 °C 1.2: 61 percent / ICH2CH2Cl / diethyl ether; pentane / 16 h / 20 °C 2.1: BBr3 / CH2Cl2 / 16 h / -78 - 20 °C View Scheme
参考文献
Dumez, Estelle; Snaith, John S.; Jackson, Richard F. W.; McElroy, Andrew B.; Overington, John; Wythes, Martin J.; Withka, Jane M.; McLellan, Thomas J.
Journal of Organic Chemistry, 2002 , vol. 67, # 14 p. 4882 - 4892
Dumez, Estelle; Snaith, John S.; Jackson, Richard F. W.; McElroy, Andrew B.; Overington, John; Wythes, Martin J.; Withka, Jane M.; McLellan, Thomas J.
Journal of Organic Chemistry, 2002 , vol. 67, # 14 p. 4882 - 4892
Dumez, Estelle; Snaith, John S.; Jackson, Richard F. W.; McElroy, Andrew B.; Overington, John; Wythes, Martin J.; Withka, Jane M.; McLellan, Thomas J.
Journal of Organic Chemistry, 2002 , vol. 67, # 14 p. 4882 - 4892