6-(羟基甲基)-2H-苯并[b][1,4]噻嗪-3(4h)-酮合成路线 （共 2 条）
反应条件
manganese(IV) oxide in tetrahydrofuran; chloroform T=70°C; 4 h;
参考文献
Allison, Brett D.; Gomez, Laurent; Grice, Cheryl A.; Hack, Michael D.; Morrow, Brian J.; Motley, S. Timothy; Santillan, Alejandro; Shaw, Karen J.; Schwarz, Kimberly L.; Tang, Liu Y.; Venkatesan, Hariharan; Wiener, John J. M.
Patent: US2006/223810 A1, 2006 ;
Location in patent: Page/Page column 22 ;
反应条件
1: With triethylamine; isobutyl chloroformate in tetrahydrofuran
T=0°C; 2 h;
2: With sodium tetrahydroborate in tetrahydrofuran; water
T=0 - 20°C; 18 h;
3: With hydrogenchloride in tetrahydrofuran; water
参考文献
Allison, Brett D.; Gomez, Laurent; Grice, Cheryl A.; Hack, Michael D.; Morrow, Brian J.; Motley, S. Timothy; Santillan, Alejandro; Shaw, Karen J.; Schwarz, Kimberly L.; Tang, Liu Y.; Venkatesan, Hariharan; Wiener, John J. M.
Patent: US2006/223810 A1, 2006 ;
Location in patent: Page/Page column 22 ;
