(2,3-二氢-[1,4]二噁英o[2,3-c]吡啶-7-基)甲醇合成路线 (共 12 条)
反应条件
1: ammonium hydroxide / 16 h / 90 °C / |Sealed tube 2: palladium 10 on activated carbon; hydrogen; sodium hydroxide / water / 16 h / 20 °C / |Inert atmosphere 3: potassium carbonate / N,N-dimethyl-formamide / 16 h / 80 °C View Scheme
反应条件
manganese(IV) oxide in dichloromethane 72 h;
参考文献
WO2006/81264 A1, ;
Page/Page column 26-27 ;