1: 3-phenyl-propionyl chloride With triethylamine in dichloromethane T=20°C; 16 h; 2: lithium phenylacetylide in tetrahydrofuran T=0°C; 1 h; 3: With hydrogenchloride in tetrahydrofuran T=0°C; 0.25 h; Further stages.;
参考文献
Hansen, Anne-Lene L.; Murray, Anthony; Tanner, David
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 24 p. 4497 - 4505
1: lithium phenylacetylide With 1,4-diiodobutane T=25°C; Alkylation; 20 h; 2: acetone T=25°C; Alkylation; Further stages.;
参考文献
Jones, Graham B.; Wright, Justin M.; Plourde, Gary W.; Hynd, George; Huber, Robert S.; Mathews, Jude E.
Journal of the American Chemical Society, 2000 , vol. 122, # 9 p. 1937 - 1944
