1-乙烯基-3,5,7,9,11,13,15-异丁基戊环-[9.5.1.13,9.15,15.17,13]八硅氧烷合成路线 （共 4 条）
反应条件
tetraethylammonium hydroxide in tetrahydrofuran; water
T=20°C;
参考文献
DEGUSSA AG
Patent: WO2006/27074 A1, 2006 ;
Location in patent: Page/Page column 14 ;
反应条件
triethylamine in pentane
T=0 - 20°C; Inert atmosphere;
参考文献
Zak, Patrycja; Pietraszuk, Cezary; Marciniec, Bogdan; Spolnik, Brzegorz; Danikiewicz, Witold
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 16 p. 2675 - 2682
反应条件
[RuHCl(CO)(PCy3)2]; copper(l) chloride in dichloromethane
6 h; Inert atmosphereReflux;
参考文献
Zak, Patrycja; Pietraszuk, Cezary; Marciniec, Bogdan; Spolnik, Brzegorz; Danikiewicz, Witold
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 16 p. 2675 - 2682
反应条件
RuCl2(tricyclohexylphosphine)2(benzylidene) in dichloromethane
6 h; Inert atmosphereReflux;
参考文献
Zak, Patrycja; Pietraszuk, Cezary; Marciniec, Bogdan; Spolnik, Brzegorz; Danikiewicz, Witold
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 16 p. 2675 - 2682
