isopentyl nitrite in tetrahydrofuran
1 h; Heating;
参考文献
Natarajan, Swaminathan R.; Wisnoski, David D.; Thompson, James E.; O'Neill, Edward A.; O'Keefe, Stephen J.
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 16 p. 4400 - 4404
1: 88 percent / aq. Cs2CO3; Pd(PPh3)4 / toluene; methanol / 12 h / Heating
2: 85 percent / Raney Ni / methanol / 7 h / 20 °C
3: 85 percent / Br2; aq. HCl / tetrahydrofuran / 2 h
4: 80 percent / i-amylONO / tetrahydrofuran / 1 h / Heating
View Scheme
参考文献
Natarajan, Swaminathan R.; Wisnoski, David D.; Thompson, James E.; O'Neill, Edward A.; O'Keefe, Stephen J.
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 16 p. 4400 - 4404
1: 88 percent / aq. Cs2CO3; Pd(PPh3)4 / toluene; methanol / 12 h / Heating
2: 85 percent / Raney Ni / methanol / 7 h / 20 °C
3: 85 percent / Br2; aq. HCl / tetrahydrofuran / 2 h
4: 80 percent / i-amylONO / tetrahydrofuran / 1 h / Heating
View Scheme
参考文献
Natarajan, Swaminathan R.; Wisnoski, David D.; Thompson, James E.; O'Neill, Edward A.; O'Keefe, Stephen J.
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 16 p. 4400 - 4404
Natarajan, Swaminathan R.; Wisnoski, David D.; Thompson, James E.; O'Neill, Edward A.; O'Keefe, Stephen J.
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 16 p. 4400 - 4404
1: 85 percent / Raney Ni / methanol / 7 h / 20 °C
2: 85 percent / Br2; aq. HCl / tetrahydrofuran / 2 h
3: 80 percent / i-amylONO / tetrahydrofuran / 1 h / Heating
View Scheme
参考文献
Natarajan, Swaminathan R.; Wisnoski, David D.; Thompson, James E.; O'Neill, Edward A.; O'Keefe, Stephen J.
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 16 p. 4400 - 4404
