2'-脱氧-3',5'-二-O-(4-甲基苯甲酰)尿苷合成路线 (共 4 条)
反应条件
pyridine
T=0 - 50°C;
参考文献
Jin, Xuanye; Yang, Ruchun; Jin, Peiyuan; Xiao, Qiang; Ju, Yong
Synthesis, 2007 , # 19 p. 2967 - 2972
反应条件
1: pyridine / 3 h / 20 °C
2: H2O / 1,2-dimethoxy-ethane / 12 h / 125 °C
View Scheme
参考文献
Nowak, Ireneusz; Robins, Morris J.
Organic Letters, 2005 , vol. 7, # 22 p. 4903 - 4905
反应条件
in pyridine
1.) 0 degC to R.T., 2.) 50 degC, 2 h;
参考文献
Robins, Morris, J.; Barr, Philip J.; Giziewicz, Jerzy
Canadian Journal of Chemistry, 1982 , vol. 60, p. 554 - 557
反应条件
tin(IV) chloride
1.) CH3CN, 80 deg C, 30 min; 2.) CH3CN, r.t.; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Janardhanam, Selvasekaran; Nambiar, Krishnan P.
Tetrahedron Letters, 1994 , vol. 35, # 22 p. 3657 - 3660