2,3,4,6-TETRA-O-ACETYL-ALPHA-D-GLUCOPYRANOSYL CHLORIDE合成路线 (共 18 条)
反应条件
pyridine; benzyl alcohol zinc salt 1.) CH2Cl2, reflux, 24 h, 2.) room temperature, 24 h; Multistep reaction. Yields of byproduct given;
参考文献
Gurudutt, Kambadoor N.; Rao, Lingamallu Jagan Mohan; Rao, Sanjay; Srinivas, Subramanian
Carbohydrate Research, 1996 , vol. 285, p. 159 - 165
反应条件
pyridine; acetic anhydride 1.) CH2Cl2, reflux, 24 h, 2.) room temperature, 24 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Gurudutt, Kambadoor N.; Rao, Lingamallu Jagan Mohan; Rao, Sanjay; Srinivas, Subramanian
Carbohydrate Research, 1996 , vol. 285, p. 159 - 165
反应条件
pyridine; benzyl alcohol zinc salt 1.) CH2Cl2, reflux, 24 h, 2.) room temperature, 24 h; Multistep reaction. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 285, p. 159 - 165
反应条件
pyridine; acetic anhydride 1.) CH2Cl2, reflux, 24 h, 2.) room temperature, 24 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 285, p. 159 - 165
反应条件
trimethylsilylazide; tetra-n-butylammonium difluorotriphenylsilicate(IV) in tetrahydrofuran T=65°C; Substitution; 20 h;
参考文献
Soli, Eric D.; DeShong, Philip
Journal of Organic Chemistry, 1999 , vol. 64, # 26 p. 9724 - 9726
反应条件
2: methanol. HCl View Scheme
参考文献
Young et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 2126,2128
参考文献
Young et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 2126,2128
反应条件
aluminium trichloride; dichloroaluminium acetate in dichloromethane 2 h; Heating;
参考文献
Rajanikanth, B.; Seshadri, R.
Tetrahedron Letters, 1987 , vol. 28, # 20 p. 2295 - 2296