1,4-二氢-1,4-甲桥萘合成路线 （共 42 条）
反应条件
magnesium in diethyl ether T=20°C; 3 h; ultrasonics;
参考文献
Fernandez, Franco; Garcia-Mera, Xerardo; Morales, Melvin; Rodriguez-Borges, Jose E.; De Clercq, Eric
Synthesis, 2002 , # 8 p. 1084 - 1090
反应条件
n-butyllithium in hexane; toluene T=0 - 20°C; Diels-Alder cycloaddition;
参考文献
Brooks, Paige R.; Caron, Stephane; Coe, Jotham W.; Ng, Karl K.; Singer, Robert A.; Vazquez, Enrique; Vetelino, Michael G.; Watson Jr., Harry H.; Whritenour, David C.; Wirtz, Michael C.
Synthesis, 2004 , # 11 p. 1755 - 1758
反应条件
lanthanum; iodine in tetrahydrofuran T=25°C; 4 h;
参考文献
Kawabata, Hiroshi; Nishino, Toshiki; Nishiyama, Yutaka; Sonoda, Noboru
Tetrahedron Letters, 2002 , vol. 43, # 28 p. 4911 - 4913
反应条件
n-butyllithium in hexane; toluene T=0 - 20°C; Diels-Alder cycloaddition;
参考文献
Coe, Jotham W.; Wirtz, Michael C.; Bashore, Crystal G.; Candler, John
Organic Letters, 2004 , vol. 6, # 10 p. 1589 - 1592
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; methyl-ethyl phosphite 6 h; Ambient temperature;
参考文献
Trost; Tometzki
Synthesis, 1991 , # 12 p. 1235 - 1245
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in chloroform 48 h; Ambient temperature;
参考文献
Cossu, Sergio; De Lucchi, Ottorino
Tetrahedron, 1996 , vol. 52, # 45 p. 14247 - 14252
反应条件
sodium; tert-butyl alcohol in tetrahydrofuran Heating;
参考文献
Hales, Neil J.; Heaney, Harry; Hollinshead, John H.; Lai, Steven M. F.; Singh, Pritpal
Tetrahedron, 1995 , vol. 51, # 28 p. 7777 - 7790
反应条件
1: 88 percent / BuLi / tetrahydrofuran; hexane / 0 - 20 °C 2: 26 percent / (i-PrO)3P / (dba)3Pd2*CHCl3 / tetrahydrofuran / 6 h / Ambient temperature View Scheme
参考文献
Trost, Barry M.; Tometzki, Gerald B.
Journal of Organic Chemistry, 1988 , vol. 53, # 4 p. 915 - 917
反应条件
in diethyl ether T=0°C; Irradiation; MechanismProduct distribution;
参考文献
Adam, Waldemar; Lucchi, Ottorino De
Journal of Organic Chemistry, 1981 , vol. 46, # 21 p. 4133 - 4138
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 2: With trimethylstannyl chloride in tetrahydrofuran; hexane T=-78 - 20°C; 3: With Cu(NO3)2*3H2O in tetrahydrofuran T=20°C;
参考文献
Nisanci, Bilal; Dalkilic, Erdin; Gueney, Murat; Dastan, Arif
Beilstein Journal of Organic Chemistry, 2009 , vol. 5, art. no. A39
