3-溴-5-(甲基磺酰)砒啶合成路线 (共 3 条)
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
反应条件
n-butyllithium; oxone in tetrahydrofuran; methanol; diethyl ether; ethyl acetate
反应条件
potassium acetate; tri-cyclo-hexyl-phosphine; tris-(dibenzylideneacetone)dipalladium(0) in 1,4-dioxane T=100°C; 5 h;
参考文献
MERCK SERONO S.A.; SWINNEN, Dominique; JORAND-LEBRUN, Catherine; GRIPPI-VALLOTTON, Tania; GERBER, Patrick; GONZALEZ, Jerome; SHAW, Jeffrey; JEYAPRAKASHNARAYANAN, Seenisamy
Patent: WO2010/100144 A1, 2010 ;
Location in patent: Page/Page column 136 ;
WO 2010/100144 A1