(甲氧基甲基)二苯基磷氧合成路线 （共 33 条）
反应条件
1: n-propyl-magnesium bromide; Ph2P(O)CH2OCH3 in tetrahydrofuran
T=20°C; Addition;
2: 4-chlorobenzaldehyde Addition;
参考文献
Cardellicchio, Cosimo; Fracchiolla, Giuseppe; Naso, Francesco; Tortorella, Paolo; Holody, Wieslawa; Michal Pietrusiewicz
Tetrahedron Letters, 1999 , vol. 40, # 31 p. 5773 - 5776
反应条件
1: n-propyl-magnesium bromide; Ph2P(O)CH2OCH3 in tetrahydrofuran
T=20°C; Substitution;
2: ortho-anisaldehyde Addition;
参考文献
Cardellicchio, Cosimo; Fracchiolla, Giuseppe; Naso, Francesco; Tortorella, Paolo; Holody, Wieslawa; Michal Pietrusiewicz
Tetrahedron Letters, 1999 , vol. 40, # 31 p. 5773 - 5776
反应条件
cupric triflate; 1,1,3,3-tetramethyldisiloxane in toluene
T=100°C; Inert atmosphere;
参考文献
Li, Yuehui; Das, Shoubhik; Zhou, Shaolin; Junge, Kathrin; Beller, Matthias
Journal of the American Chemical Society, 2012 , vol. 134, # 23 p. 9727 - 9732
反应条件
lithium diisopropyl amide
1) THF, 0 deg C, 10 min, 2) -78 deg C, 5 min; Yield given. Multistep reaction;
参考文献
Huby, Nicholas J. S.; Kinsman, Richard G.; Lathbury, David; Vernon, Peter G.; Gallagher, Timothy
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 1 p. 145 - 155
反应条件
in tetrahydrofuran
T=20°C; Substitution; 40 h;
参考文献
Cardellicchio, Cosimo; Fracchiolla, Giuseppe; Naso, Francesco; Tortorella, Paolo; Holody, Wieslawa; Michal Pietrusiewicz
Tetrahedron Letters, 1999 , vol. 40, # 31 p. 5773 - 5776
反应条件
in tetrahydrofuran
T=20°C; Substitution; 5 h;
参考文献
Cardellicchio, Cosimo; Fracchiolla, Giuseppe; Naso, Francesco; Tortorella, Paolo; Holody, Wieslawa; Michal Pietrusiewicz
Tetrahedron Letters, 1999 , vol. 40, # 31 p. 5773 - 5776
反应条件
in tetrahydrofuran
T=20°C; Substitution; 2 h;
参考文献
Cardellicchio, Cosimo; Fracchiolla, Giuseppe; Naso, Francesco; Tortorella, Paolo; Holody, Wieslawa; Michal Pietrusiewicz
Tetrahedron Letters, 1999 , vol. 40, # 31 p. 5773 - 5776
反应条件
in tetrahydrofuran
T=20°C; Substitution; 15 h;
参考文献
Cardellicchio, Cosimo; Fracchiolla, Giuseppe; Naso, Francesco; Tortorella, Paolo; Holody, Wieslawa; Michal Pietrusiewicz
Tetrahedron Letters, 1999 , vol. 40, # 31 p. 5773 - 5776
反应条件
in tetrahydrofuran
T=20°C; Substitution; 3 h;
参考文献
Cardellicchio, Cosimo; Fracchiolla, Giuseppe; Naso, Francesco; Tortorella, Paolo; Holody, Wieslawa; Michal Pietrusiewicz
Tetrahedron Letters, 1999 , vol. 40, # 31 p. 5773 - 5776
反应条件
in tetrahydrofuran
T=20°C; Substitution; 2 h;
参考文献
Cardellicchio, Cosimo; Fracchiolla, Giuseppe; Naso, Francesco; Tortorella, Paolo; Holody, Wieslawa; Michal Pietrusiewicz
Tetrahedron Letters, 1999 , vol. 40, # 31 p. 5773 - 5776
