3-甲基-1,5-戊二醇合成路线 （共 33 条）
反应条件
sodium hydroxide; hydrogen; nickel in water T=120°C; P=6600.66 Torr; pH=8.4 - 10.9; 5 h; Product distribution / selectivity;
参考文献
Kuraray Co., Ltd.
Patent: EP2017248 A1, 2009 ;
Location in patent: Page/Page column 5-6 ;
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 4 h; Heating;
参考文献
Harusawa, Shinya; Takemura, Shigetaka; Osaki, Hirotaka; Yoneda, Ryuji; Kurihara, Takushi
Tetrahedron, 1993 , vol. 49, # 35 p. 7657 - 7666
反应条件
hydrogen; copper T=240°C; P=225018 Torr; 5 h;
参考文献
Devekki, A. V.; Koshelev, Yu. N.; Malov, Yu. I.; Devekki, A. B.; Strashnova, G. M.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 11 p. 2652 - 2653,2392 - 2393
反应条件
copper oxide-chromium oxide; water; hydrogen T=180°C; P=144160 Torr;
参考文献
Shell Devel.Co.
Patent: US2546019 , 1947 ;
反应条件
borane-THF 18 h; Heating;
参考文献
Equi, Angela M.; Brown, Alison M.; Cooper, Alan; Her, Surjit K.; Watson, Allan B.; Robins, David J.
Tetrahedron, 1991 , vol. 47, # 3 p. 507 - 518
反应条件
manganese(IV) dioxide; copper (II) chromite
参考文献
Kuraray Company, Ltd.
Patent: US4663468 A1, 1987 ;
反应条件
lithium aluminium tetrahydride
参考文献
Rozen, Shlomo; Gal, Chava
Journal of Organic Chemistry, 1987 , vol. 52, # 22 p. 4928 - 4933
反应条件
copper oxide-chromium oxide Hydrogenation;
参考文献
Karrer; Lee
Helvetica Chimica Acta, 1934 , vol. 17, p. 547
反应条件
ethanol; nickel T=100°C; P=36775.4 Torr; Hydrogenation;
参考文献
Ashley et al.
Journal of the Chemical Society, 1958 , p. 3298,3308
反应条件
1,4-dioxane; nickel T=100°C; P=257428 Torr; Hydrogenation;
参考文献
Du Pont de Nemours and Co.
Patent: US2789996 , 1953 ;
