3-甲基-1,5-戊二醇合成路线 （共 33 条）
反应条件
1.1: CuI / tetrahydrofuran / 20 °C 1.2: TMSCl / tetrahydrofuran / -78 - 20 °C 2.1: lithium aluminum hydride / tetrahydrofuran / 24 h / Heating View Scheme
参考文献
Chang, Chih-Shiang; Lin, Ying-Ting; Shih, Shin-Ru; Lee, Chung-Chi; Lee, Yen-Chun; Tai, Chia-Liang; Tseng, Sung-Nien; Chern, Jyh-Haur
Journal of Medicinal Chemistry, 2005 , vol. 48, # 10 p. 3522 - 3535
参考文献
Blomquist; Verdol
Journal of the American Chemical Society, 1955 , vol. 77, p. 78
反应条件
T=250°C; P=147102 - 220652 Torr;
参考文献
Wojcik; Adkins
Journal of the American Chemical Society, 1933 , vol. 55, p. 4943
反应条件
1: H2 / Co2(CO)8 / 140 °C / 132391 Torr 2: LiAlH4 View Scheme
参考文献
Derbesy,M. et al.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1971 , vol. 272, p. 86 - 88
反应条件
hydrogenchloride und Hydrieren des Reaktionsgemisches an Raney-Nickel in neutraler Loesung bei 125grad;
参考文献
Longley; Emerson
Organic Syntheses, 1954 , vol. 34, p. 71
反应条件
lithium aluminium tetrahydride
参考文献
Derbesy,M. et al.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1971 , vol. 272, p. 86 - 88
反应条件
1: aqueous sulfuric acid 2: Raney nickel; ethanol / 100 °C / 36775.4 Torr / Hydrogenation View Scheme
参考文献
Ashley et al.
Journal of the Chemical Society, 1958 , p. 3298,3308
反应条件
1: 200 °C 2: Raney nickel; dioxane / 100 °C / 257428 Torr / Hydrogenation View Scheme
参考文献
Du Pont de Nemours and Co.
Patent: US2789996 , 1953 ;
反应条件
VTi2P5.1O(x) T=350°C; 3 h; Catalytic behavior;
参考文献
Eastman Chemical Company; Norman, David William
Patent: US2013/72696 A1, 2013 ;
Location in patent: Paragraph 0042; 0046 ;
反应条件
1,4-dioxane; copper oxide-chromium oxide; hydrogen T=250°C; P=147102 - 294203 Torr;
参考文献
Paden; Adkins
Journal of the American Chemical Society, 1936 , vol. 58, p. 2493
