2,4-二氟-1-硝基苯合成路线 (共 113 条)
反应条件
trihexyl (tetradecyl) phosphonium tetrafluoroborate; potassium fluoride in dimethyl sulfoxide T=180°C; 1.8 h;
参考文献
Fan, Ao; Chuah, Gaik-Khuan; Jaenicke, Stephan
Catalysis Today, 2012 , vol. 198, # 1 p. 300 - 304
反应条件
potassium fluoride; water; anhydrous tetramethylammonium chloride in acetic acid T=120°C; 3.5 h;
参考文献
Sasson, Yoel; Negussie, Samuel; Royz, Michael; Mushkin, Noam
Chemical Communications, 1996 , # 3 p. 297 - 298
反应条件
potassium fluoride; [bis(triphenyl-λ5-phosphanylidene)ammonium][Cl] in dimethyl sulfoxide T=150°C; 8 h; Inert atmosphere;
参考文献
Lacour, Marie-Agnes; Zablocka, Maria; Duhayon, Carine; Majoral, Jean-Pierre; Taillefer, Marc
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 17 p. 2677 - 2682
反应条件
potassium fluoride in anhydrous xylene
参考文献
Hoechst Aktiengesellschaft
Patent: US5502260 A1, 1996 ;
反应条件
water; fluorine in acetonitrile T=20°C; 5 h; Inert atmosphereFlow reactor;
参考文献
McPake, Christopher B.; Murray, Christopher B.; Sandford, Graham
ChemSusChem, 2012 , vol. 5, # 2 p. 312 - 319
反应条件
potassium fluoride; anhydrous tetramethylammonium chloride in anhydrous xylene
参考文献
Hoechst Aktiengesellschaft
Patent: US5502260 A1, 1996 ;
反应条件
potassium fluoride; anhydrous tetramethylammonium chloride in sulfolane T=170°C; 4 h; Product distribution / selectivity;
参考文献
Laurain, Nathalie; Zard, Samir
Patent: US2004/24238 A1, 2004 ;
Location in patent: Page 5 ;
反应条件
potassium fluoride in anhydrous xylene
参考文献
Hoechst Aktiengesellschaft
Patent: US5502260 A1, 1996 ;
参考文献
Rhone-Poulenc Chimie
Patent: US5354439 A1, 1994 ;
参考文献
Hoechet AG
Patent: US5545768 A1, 1996 ;