5-溴-2-甲氧基吡啶1-氧化物合成路线 （共 3 条）
反应条件
triethylamine in acetonitrile T=80°C; 15 h; Inert atmosphere;
参考文献
F. HOFFMANN-LA ROCHE AG; GENENTECH, INC; CHEN, Huifen; CRAWFORD, Terry; MAGNUSON, Steven, R.; NDUBAKU, Chudi; WANG, Lan
Patent: WO2013/113669 A1, 2013 ;
Location in patent: Page/Page column 74 ;
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=40°C; 16 h; Inert atmosphere;
参考文献
F. HOFFMANN-LA ROCHE AG; GENENTECH, INC; CHEN, Huifen; CRAWFORD, Terry; MAGNUSON, Steven, R.; NDUBAKU, Chudi; WANG, Lan
Patent: WO2013/113669 A1, 2013 ;
Location in patent: Page/Page column 74 ;
反应条件
sulfuric acid; nitric acid in water
T=80°C; 14 h;
参考文献
Wang, Tao; Zhang, Zhongxing; Meanwell, Nicholas A.; Kadow, John F.; Yin, Zhiwei; Xue, Qiufen May; Regueiro-Ren, Alicia; Matiskella, John D.; Ueda, Yasutsugu
Patent: US2004/110785 A1, 2004 ;
Location in patent: Page 76 ;
