2-(4-甲基苯基)吡啶合成路线 （共 103 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; lithium chloride in toluene T=110°C; 10 h; Inert atmosphere;
参考文献
Tang, Jian-Hong; Wu, Si-Hai; Shao, Jiang-Yang; Nie, Hai-Jing; Zhong, Yu-Wu
Organometallics, 2013 , vol. 32, # 16 p. 4564 - 4570
反应条件
tetrakis(triphenylphosphine) palladium(0); copper(I) thiophene-2-carboxylate; acetic acid in water T=50°C; 24 h;
参考文献
Koley, Moumita; Wimmer, Laurin; Schnuerch, Michael; Mihovilovic, Marko D.
Journal of Heterocyclic Chemistry, 2013 , vol. 50, # 6 p. 1368 - 1373
反应条件
C60H48Cl2FeP4 in tetrahydrofuran; toluene T=100°C; Negishi coupling reaction; 4 h; Inert atmosphere;
参考文献
Bedford, Robin B.; Hall, Mark A.; Hodges, George R.; Huwe, Michael; Wilkinson, Mark C.
Chemical Communications, 2009 , # 42 p. 6430 - 6432
反应条件
C60H48Cl2FeP4 in tetrahydrofuran; toluene T=100°C; Negishi coupling reaction; 4 h; Inert atmosphere;
参考文献
Bedford, Robin B.; Hall, Mark A.; Hodges, George R.; Huwe, Michael; Wilkinson, Mark C.
Chemical Communications, 2009 , # 42 p. 6430 - 6432
反应条件
C52H44CoN4O4; potassium hydroxide; tert-butyl alcohol T=200°C; 10 h; Inert atmosphereDarkness;
参考文献
Tetrahedron Letters, , vol. 53, # 13 p. 1571 - 1575
反应条件
copper(I) oxide; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; palladium dichloride in N,N-dimethyl acetamide T=150°C; 24 h; Inert atmosphereMolecular sieve;
参考文献
Li, Xinjian; Zou, Dapeng; Leng, Faqiang; Sun, Chunxia; Li, Jingya; Wu, Yangjie; Wu, Yusheng
Chemical Communications, 2013 , vol. 49, # 3 p. 312 - 314
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; potassium carbonate in neat (no solvent) T=110°C; Suzuki-Miyaura Coupling; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Asachenko, Andrey F.; Sorochkina, Kristina R.; Dzhevakov, Pavel B.; Topchiy, Maxim A.; Nechaev, Mikhail S.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3553 - 3557
反应条件
2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane T=80°C; 32 h;
参考文献
Organic Letters, , vol. 2, # 24 p. 3933 - 3935
反应条件
tris-(dibenzylideneacetone)dipalladium(0); copper(I) bromide dimethylsulfide complex; trifuran-2-yl-phosphane in tetrahydrofuran Stille coupling; Heating;
参考文献
Dubbaka, Srinivas Reddy; Vogel, Pierre
Journal of the American Chemical Society, 2003 , vol. 125, # 50 p. 15292 - 15293
反应条件
1: 1-(iodo)-4-methylbenzene With methyllithium; zinc(II) chloride in tetrahydrofuran; diethyl ether T=-78°C; 2 h; 2: 2-methoxy-pyridine With bis(1,5-cyclooctadiene)nickel (0); tri-cyclo-hexyl-phosphine in toluene T=20°C; Negishi coupling reaction; 12 h; Inert atmosphere;
参考文献
Wang, Chao; Ozaki, Takashi; Takita, Ryo; Uchiyama, Masanobu
Chemistry - A European Journal, 2012 , vol. 18, # 12 p. 3482 - 3485
