2-(4-甲基苯基)吡啶合成路线 (共 103 条)
反应条件
copper(l) iodide; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=100°C; 22 h; Inert atmosphere;
参考文献
Heterocycles, , vol. 80, # 1 p. 359 - 368
反应条件
palladium diacetate; potassium carbonate; triphenylphosphine in toluene 12 h; RefluxInert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 15, # 47 p. 13105 - 13110
反应条件
dipotassium peroxodisulfate; silver nitrate; trifluoroacetic acid in dichloromethane; water T=23°C; 3 h;
参考文献
Seiple, Ian B.; Su, Shun; Rodriguez, Rodrigo A.; Gianatassio, Ryan; Fujiwara, Yuta; Sobel, Adam L.; Baran, Phil S.
Journal of the American Chemical Society, 2010 , vol. 132, # 38 p. 13194 - 13196
反应条件
1: triethylamine / tetrahydrofuran / 18 h / 0 - 20 °C / |Inert atmosphere 2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol / 18 h / 100 °C / |Inert atmosphere View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 12, # 1 p. 47 - 52
反应条件
trifluoroacetic acid T=65 - 70°C; 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 50, # 13 p. 2232 - 2235
反应条件
tricyclohexylphosphine-Au(I); potassium tert-butylate T=100°C; 24 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 50, # 13 p. 1478 - 1481
反应条件
potassium acetate; 18-crown-6 ether 1.5 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 49, # 9 p. 1594 - 1603
反应条件
anthracene 2 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 46, # 22 p. 4567 - 4569
反应条件
palladium on activated charcoal; 4-allyl-1,2-methylenedioxybenzene T=190°C;
参考文献
Yakugaku Zasshi, , vol. 77, p. 490,492
Chem.Abstr., , p. 14720
反应条件
2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane; acetic acid T=80°C; 32 h;
参考文献
Tetrahedron, , vol. 60, # 29 p. 6217 - 6224