2-(4-甲基苯基)吡啶合成路线 （共 103 条）
反应条件
1: dichloromethane / 12 h / 50 °C / Inert atmosphere 2: Ni(PCy3)2Cl2 / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 8 h / 90 °C / Inert atmosphere View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 21 p. 4901 - 4904
反应条件
1: hydrogenchloride / water / 20 °C / |Inert atmosphere; |Schlenk technique 2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene; ethanol / 20 h / |Inert atmosphere; |Schlenk technique; |Reflux View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 4 p. 1264 - 1267
反应条件
1: 1.) 1 M aq. HCl, NaNO2 / 1.) 0 deg C, 30 min, 2.) 0 deg C, 30 min 2: CF3COOH / 3 h / 65 - 70 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 50, # 13 p. 2232 - 2235
反应条件
1: [(t-Bu)3PH]BF4; potassium carbonate; palladium diacetate / toluene / 16 h / 110 °C / |Sealed tube; |Inert atmosphere 2: tetrahydroxydiboron / N,N-dimethyl-formamide; acetonitrile / 0.17 h / 20 °C View Scheme
参考文献
Synlett, , vol. 24, # 20 art. no. ST-2013-S0695-L, p. 2695 - 2700
参考文献
Furukawa, Naomichi; Tsuruoka, Masayuki; Fujihara, Hisashi
Heterocycles, 1986 , vol. 24, # 12 p. 3337 - 3340
反应条件
in dichloromethane 15 h; Ambient temperatureIrradiation; Yield given. Yields of byproduct given;
参考文献
Terashima, Masanao; Seki, Koh-ichi; Yoshida, Chihiro; Ohkura, Kazue; Kanaoka, Yuichi
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 3 p. 1009 - 1015
反应条件
2: soda lime / 280 °C 3: palladium/charcoal; safrole / 190 °C View Scheme
参考文献
Yakugaku Zasshi, , vol. 77, p. 490,492
Chem.Abstr., , p. 14720
反应条件
1: soda lime / 280 °C 2: palladium/charcoal; safrole / 190 °C View Scheme
参考文献
Yakugaku Zasshi, , vol. 77, p. 490,492
Chem.Abstr., , p. 14720
反应条件
Br(1-)*C18H28N3(1+); sodium t-butanolate T=110°C; 4 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 48, # 53 p. 6702 - 6704
反应条件
200 h; Ambient temperatureIrradiationisotope effects; other p-tolyl radical sources;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 54, # 8 p. 2535 - 2536
