反应条件
hydrogenchloride; lithium hydroxide; sodium hydrogencarbonate; triethylamine; phenyl chlorothione carbonate 1.) H2O, THF, room temperature, 2 h, 2.) room temperature, 4 h, 3.) MeOH, room temperature, 16 h, 4.) THF, H2O, room temperature, 18 h, 5.) CH2Cl2, room temperature, 15 min; Yield given. Multistep reaction;
参考文献
Xu; Yadan
Journal of Organic Chemistry, 1995 , vol. 60, # 20 p. 6296 - 6301
