2-氯-2-苯基苯乙酮合成路线 (共 108 条)
反应条件
sodium hypochlorite; water in dichloromethane T=20°C; 0.5 h;
参考文献
Ruan, Libo; Shi, Min; Li, Nian; Ding, Xu; Yang, Fan; Tang, Jie
Organic Letters, 2014 , vol. 16, # 3 p. 733 - 735
反应条件
oxygen; iron(III) chloride in pyridine 0.5 h; Irradiation;
参考文献
Kohda, Akira; Ueda, Keiko,; Sato, Tadashi
Journal of Organic Chemistry, 1981 , vol. 46, # 3 p. 509 - 515
反应条件
1: boron trifluoride diethyl etherate / dichloromethane / 20 °C 2: sodium hypochlorite; water / dichloromethane / 4 h / 20 °C View Scheme
参考文献
Ruan, Libo; Shi, Min; Li, Nian; Ding, Xu; Yang, Fan; Tang, Jie
Organic Letters, 2014 , vol. 16, # 3 p. 733 - 735
反应条件
1.1: sodium hydroxide / ethanol; water / 20 °C 1.2: 0 - 20 °C 2.1: boron trifluoride diethyl etherate / dichloromethane / 20 °C 3.1: sodium hypochlorite; water / dichloromethane / 4 h / 20 °C View Scheme
参考文献
Ruan, Libo; Shi, Min; Li, Nian; Ding, Xu; Yang, Fan; Tang, Jie
Organic Letters, 2014 , vol. 16, # 3 p. 733 - 735
反应条件
ethanol; hydrogen; platinum
参考文献
Buck; Ide
Journal of the American Chemical Society, 1932 , vol. 54, p. 4359,4364
反应条件
1: PCl5 2: ethanol; platinum; hydrogen View Scheme
参考文献
Buck; Ide
Journal of the American Chemical Society, 1932 , vol. 54, p. 4359,4364
反应条件
1: boron trifluoride diethyl etherate / dichloromethane / 20 °C 2: sodium hypochlorite; water / dichloromethane / 0.5 h / 20 °C View Scheme
参考文献
Ruan, Libo; Shi, Min; Li, Nian; Ding, Xu; Yang, Fan; Tang, Jie
Organic Letters, 2014 , vol. 16, # 3 p. 733 - 735
反应条件
1.1: sodium hydroxide / ethanol; water / 20 °C 1.2: 0 - 20 °C 2.1: boron trifluoride diethyl etherate / dichloromethane / 20 °C 3.1: sodium hypochlorite; water / dichloromethane / 0.5 h / 20 °C View Scheme
参考文献
Ruan, Libo; Shi, Min; Li, Nian; Ding, Xu; Yang, Fan; Tang, Jie
Organic Letters, 2014 , vol. 16, # 3 p. 733 - 735
反应条件
1: P2O5 2: 70 percent / PCC / CH2Cl2 / 6 h / Ambient temperature View Scheme
参考文献
Wilson, R. Marshall; Chow, Tahsin J.
Tetrahedron Letters, 1983 , vol. 24, # 43 p. 4635 - 4636
反应条件
1: Perkin condensation 2: 5 percent / manganese(III)acetate, LiCl / acetic acid / 0.67 h / Heating 3: 80 percent / manganese(II)acetate, acetic anhydride / acetic acid / 3 h / Heating View Scheme
参考文献
Yonemura, Hiroshi; Nishino, Hiroshi; Kurosawa, Kazu
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 3153 - 3160