4-[2,2':6',2''-三联吡啶]-4'-基-苯甲醇合成路线 （共 5 条）
反应条件
1: With sodium hydroxide
T=0°C; 2 h;
2: With ammonia in water
T=100°C; 2 h;
参考文献
Goldstein, Daniel C.; Peterson, Joshua R.; Cheng, Yuen Yap; Clady, Raphael G.C.; Schmidt, Timothy W.; Thordarson, Pall
Molecules, 2013 , vol. 18, # 8 p. 8959 - 8975
反应条件
sodium hydrogencarbonate in water; acetonitrile
参考文献
Anthonysamy, Arockiam; Balasubramanian, Sengottuvelan; Shanmugaiah, Vellasamy; Mathivanan, Narayanasamy
Dalton Transactions, 2008 , # 16 p. 2136 - 2143
反应条件
1.1: sodium tetrahydroborate / tetrahydrofuran / 0 - 20 °C
2.1: sodium hydroxide / 2 h / 0 °C
2.2: 2 h / 100 °C
View Scheme
参考文献
Hvasanov, David; Mason, Alexander F.; Goldstein, Daniel C.; Bhadbhade, Mohan; Thordarson, Pall
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 28 p. 4602 - 4612
反应条件
1: NaOH / various solvent(s) / 2 h / 0 °C
2: aq. NH3 / various solvent(s) / 2 h / 100 °C
View Scheme
参考文献
Winter, Andreas; Van Den Berg, Antje M. J.; Hoogenboom, Richard; Kickelbick, Guido; Schubert, Ulrich S.
Synthesis, 2006 , # 17 p. 2873 - 2878
反应条件
1: NaOH / various solvent(s) / 2 h / 0 °C
2: aq. NH3 / various solvent(s) / 2 h / 100 °C
View Scheme
参考文献
Winter, Andreas; Van Den Berg, Antje M. J.; Hoogenboom, Richard; Kickelbick, Guido; Schubert, Ulrich S.
Synthesis, 2006 , # 17 p. 2873 - 2878
