1,2:3,4-二-o-异亚丙基-6-o-对甲苯磺酰基-alpha-D-半乳糖合成路线 (共 25 条)
反应条件
sodium azide in dimethyl sulfoxide T=160°C; 2 h;
参考文献
Joosten, John A. F.; Evers, Britta; Van Summeren, Ruben P.; Kamerling, Johannis P.; Vliegenthart, Johannes F. G.
European Journal of Organic Chemistry, 2003 , # 18 p. 3569 - 3586
反应条件
lithium triethylborohydride in tetrahydrofuran Heating;
参考文献
Thiem; Meyer
Chemische Berichte, 1980 , vol. 113, # 9 p. 3067 - 3074
反应条件
[Mg2Cl3(THF)y]+*[AlH4-nCln]- in tetrahydrofuran T=70°C; Reduction; 72 h;
参考文献
Szabovik; Medgyes; Antal; Varga; Knott; Liptak
Polish Journal of Chemistry, 1999 , vol. 73, # 6 p. 1003 - 1009
反应条件
1: benzene; lithium alanate; diethyl ether 2: aqueous sulfuric acid View Scheme
参考文献
Schmid; Karrer
Helvetica Chimica Acta, 1949 , vol. 32, p. 1371,1376
反应条件
sodium hydroxide in methanol 1 h; Irradiationvarious time, also with DABCO, and in the presence of oxygen; Product distribution;
参考文献
Berki; Binkley; Hehemann; Koholic; Masnovi
Journal of Carbohydrate Chemistry, 1996 , vol. 15, # 1 p. 33 - 40
反应条件
[Mg2Cl3(THF)y]+*[AlH4-nCln]- in tetrahydrofuran T=70°C; Reduction; 72 h;
参考文献
Polish Journal of Chemistry, , vol. 73, # 6 p. 1003 - 1009
反应条件
1,4-diaza-bicyclo[2.2.2]octane in methanol Irradiationdirect evidence for electron transfer by examining flash photolysis; Mechanism;
参考文献
Berki; Binkley; Hehemann; Koholic; Masnovi
Journal of Carbohydrate Chemistry, 1996 , vol. 15, # 1 p. 33 - 40
反应条件
copper(l) iodide; 2-propenylmagnesium bromide in diethyl ether 48 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Journal of Carbohydrate Chemistry, , vol. 13, # 6 p. 841 - 850
反应条件
copper(l) iodide in diethyl ether 48 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Journal of Carbohydrate Chemistry, , vol. 13, # 6 p. 841 - 850
反应条件
sodium hydroxide in methanol 1 h; Irradiationvarious time, also with DABCO, and in the presence of oxygen; Product distribution;
参考文献
Berki; Binkley; Hehemann; Koholic; Masnovi
Journal of Carbohydrate Chemistry, 1996 , vol. 15, # 1 p. 33 - 40