3,4-环氧-4-甲基戊烷-2-酮合成路线 （共 12 条）
反应条件
[C4mim][OH] T=20°C; 0.25 h;
参考文献
Ranu, Brindaban C.; Mandal, Tanmay; Banerjee, Subhash; Dey, Suvendu S.
Australian Journal of Chemistry, 2007 , vol. 60, # 4 p. 278 - 283
参考文献
House; Wasson
Journal of the American Chemical Society, 1956 , vol. 78, p. 4394,4397
反应条件
boron trifluoride diethyl etherate; sodium iodide in acetonitrile T=-10°C; 0.0166667 h;
参考文献
Mandal, Arun K.; Mahajan, S. W.
Tetrahedron, 1988 , vol. 44, # 8 p. 2293 - 2300
反应条件
samarium diiodide in tetrahydrofuran; methanol T=-90°C; 0.0833333 h;
参考文献
Molander, Gary A.; Hahn, Gregory
Journal of Organic Chemistry, 1986 , vol. 51, # 13 p. 2596 - 2599
反应条件
T=135°C; im Autoklaven;
参考文献
Pastureau; Bader
Roczniki Chemii, 1927 , vol. 7, p. 103
反应条件
T=100°C; P=77228.3 Torr; Hydrogenation;
参考文献
Bergmann
Journal of Applied Chemistry, 1951 , vol. 1, p. 380
反应条件
1: 1) NaH / 1) dioxane, 2) 12h, reflux 2: 1) 2N H2SO4, 2) hexamethyldisilazane / 1) acetone, 24h, 2) pyridine, 12h; 5h, 80 deg C 3: 97 percent / 2N H2SO4 / diethyl ether / 12 h 4: 20 percent / POCl3 / pyridine / 24 h / 70 °C 5: 58 percent / Zn / acetic acid / 72 h / 40 °C View Scheme
参考文献
Bardili, Burkhart; Marschall-Weyerstahl, Helga; Weyerstahl, Peter
Liebigs Annalen der Chemie, 1985 , # 2 p. 275 - 300
反应条件
nitrosyl chloride in hexane
参考文献
Sergeev,G.B. et al.
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, p. 506 - 513,499 - 504
反应条件
boron trifluoride in dichloromethane
T=0 - 5°C; 1 h; Yields of byproduct given;
参考文献
Bubel', O. N.; Tishchenko, I. G.; Ptashnikov, Yu. L.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 8 p. 773 - 775
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 8 p. 1022 - 1024
反应条件
boron trifluoride diethyl etherate
Yields of byproduct given;
参考文献
Bubel', O. N.; Tishchenko, I. G.; Ptashnikov, Yu. L.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 8 p. 773 - 775
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 8 p. 1022 - 1024
