2-甲酰基氨基丙烯酸甲酯合成路线 （共 12 条）
反应条件
cesium fluoride in acetonitrile T=20°C; 18 h; Inert atmosphere;
参考文献
Blackburn, Tom; Ramtohul, Yeeman K.
Synlett, 2008 , # 8 p. 1159 - 1164
反应条件
potassium carbonate; triethylamine
T=20°C;
参考文献
Panella, Lavinia; Aleixandre, Alicia Marco; Kruidhof, Gerlof J.; Robertus, Jort; Feringa, Ben L.; De Vries, Johannes G.; Minnaard, Adriaan J.
Journal of Organic Chemistry, 2006 , vol. 71, # 5 p. 2026 - 2036
反应条件
triethylamine; p-toluenesulfonyl chloride in chloroform
0.166667 h; Ambient temperature;
参考文献
Kolasa, Teodozyj
Synthesis, 1983 , # 7 p. 539
反应条件
trimethylsilyl trifluoromethanesulfonate; 1-(Trimethylsilyl)cyclohex-2-ene in dichloromethane
1.) -78 deg C, 15 min, 2.) r.t., 2 h;
参考文献
Roos; Lopez; Brook; Hiemstra; Speckamp
Journal of Organic Chemistry, 1993 , vol. 58, # 12 p. 3259 - 3268
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
1.) -78 deg C, 15 min, 2.) r.t., 6 d;
参考文献
Roos; Lopez; Brook; Hiemstra; Speckamp
Journal of Organic Chemistry, 1993 , vol. 58, # 12 p. 3259 - 3268
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
1.) -78 deg C, 15 min, 2.) r.t., 5 d;
参考文献
Roos; Lopez; Brook; Hiemstra; Speckamp
Journal of Organic Chemistry, 1993 , vol. 58, # 12 p. 3259 - 3268
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
1.) -78 deg C, 15 min, 2.) r.t., 4 h;
参考文献
Roos; Lopez; Brook; Hiemstra; Speckamp
Journal of Organic Chemistry, 1993 , vol. 58, # 12 p. 3259 - 3268
反应条件
T=95°C; 1 h; Yield given;
参考文献
Chancellor; Morton
Synthesis, 1994 , # 10 p. 1023 - 1025
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
1.) -78 deg C, 15 min, 2.) r.t., 30 h;
参考文献
Roos; Lopez; Brook; Hiemstra; Speckamp
Journal of Organic Chemistry, 1993 , vol. 58, # 12 p. 3259 - 3268
反应条件
dimethylammonium chloride; hydroquinone
参考文献
Hellmann et al.
Chemische Berichte, 1958 , vol. 91, p. 2427,2429
