苯并[d][1,3,2]二噻唑 1,1,3,3-四氧化物合成路线 （共 63 条）
反应条件
palladium diacetate; dimethyl sulfoxide
T=35°C; Sonogashira Cross-Coupling; 1.5 h;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano
European Journal of Organic Chemistry, 2014 , vol. 2014, # 3 p. 598 - 605
反应条件
palladium diacetate; dimethyl sulfoxide
T=35°C; Sonogashira Cross-Coupling; 2 h;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano
European Journal of Organic Chemistry, 2014 , vol. 2014, # 3 p. 598 - 605
反应条件
palladium diacetate; dimethyl sulfoxide
T=35°C; Sonogashira Cross-Coupling; 2 h;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano
European Journal of Organic Chemistry, 2014 , vol. 2014, # 3 p. 598 - 605
反应条件
sodium hydride in tetrahydrofuran
Ambient temperature;
参考文献
Carlsen, Per H.J.
Tetrahedron Letters, 1998 , vol. 39, # 13 p. 1799 - 1802
反应条件
palladium diacetate; dimethyl sulfoxide
T=35°C; Sonogashira Cross-Coupling; 3 h;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano
European Journal of Organic Chemistry, 2014 , vol. 2014, # 3 p. 598 - 605
反应条件
palladium diacetate; dimethyl sulfoxide
T=35°C; Sonogashira Cross-Coupling; 2 h;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano
European Journal of Organic Chemistry, 2014 , vol. 2014, # 3 p. 598 - 605
反应条件
sodium hydride in tetrahydrofuran
Ambient temperature;
参考文献
Carlsen, Per H.J.
Tetrahedron Letters, 1998 , vol. 39, # 13 p. 1799 - 1802
反应条件
in tetrahydrofuran
T=20 - 25°C;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano; Ghigo, Giovanni
European Journal of Organic Chemistry, 2008 , # 5 p. 862 - 868
反应条件
1: 99.7 percent / PCl5 / 1.) 110 deg C, 10 min; 110 to 170 deg C, 10 min, 2.) 170 deg C, 30 min
2: 84 percent / NH3 / ethanol; benzene / 2 h / Ambient temperature
View Scheme
参考文献
Davis, Franklin A.; Han, Wei; Murphy, Christopher K.
Journal of Organic Chemistry, 1995 , vol. 60, # 15 p. 4730 - 4737
反应条件
1: 1.) aq. KMnO4, 2.) PCl5 / 1.) 90 deg C, 10 min, 2.) 110-170 deg C
2: NH3 / ethanol / 0 °C
View Scheme
参考文献
Davis, Franklin A.; Sundarababu, Gajendran; Qi, Hongyan
Organic Preparations and Procedures International, 1998 , vol. 30, # 1 p. 107 - 109
