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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
44855-57-4
合成路线
（共 30 条）
44855-57-4
+
3852-09-3
3-甲氧基丙酸甲酯
→
反应条件
34566-04-6
(S)-2-氨基辛烷
+
693-16-3
(±)-4-氨基辛烷
+
1322805-09-3
反应条件
supported Candida antartica lipase B in tert-butyl methyl ether T=38 - 40°C; 2.5 h; Molecular sieveEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Poulhes, Florent; Vanthuyne, Nicolas; Bertrand, Michele P.; Gastaldi, Stephane; Gil, Gerard
Journal of Organic Chemistry, 2011 , vol. 76, # 17 p. 7281 - 7286
44855-57-4
+
72-19-5
L-苏氨酸
→
反应条件
693-16-3
(±)-4-氨基辛烷
+
1492-24-6
L-2-氨基丁酸
+
111-13-7
反应条件
(S)-selective ω-transaminase from Ochrobactrum anthropi; L-threonine deaminase from Escherichia coli; pyridoxal 5'-phosphate T=37°C; pH=7.5; 24 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Malik, M. Shaheer; Park, Eul-Soo; Shin, Jong-Shik
Green Chemistry, 2012 , vol. 14, # 8 p. 2137 - 2140
44855-57-4
+
72-19-5
L-苏氨酸
→
反应条件
34566-04-6
(S)-2-氨基辛烷
+
693-16-3
(±)-4-氨基辛烷
+
1492-24-6
L-2-氨基丁酸
+
111-13-7
反应条件
(S)-selective ω-transaminase from Ochrobactrum anthropi; L-threonine deaminase from Escherichia coli; pyridoxal 5'-phosphate T=37°C; pH=7.5; 24 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Malik, M. Shaheer; Park, Eul-Soo; Shin, Jong-Shik
Green Chemistry, 2012 , vol. 14, # 8 p. 2137 - 2140
44855-57-4
→
反应条件
24301-94-8
反应条件
hydrogenchloride in dichloromethane; water
参考文献
Nugent, Thomas C.; Negru, Daniela E.; El-Shazly, Mohamed; Hu, Dan; Sadiq, Abdul; Bibi, Ahtaram; Umar, M. Naveed
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2085 - 2092
44855-57-4
→
反应条件
111-13-7
反应条件
potassium hydroxide in ethyl acetate T=-78°C; Product distribution;
参考文献
Hoffman, Robert V.; Kumar, Anil
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 4011 - 4014
44855-57-4
+
72-19-5
L-苏氨酸
→
反应条件
693-16-3
(±)-4-氨基辛烷
+
1492-24-6
L-2-氨基丁酸
+
111-13-7
反应条件
(S)-selective ω-transaminase from Ochrobactrum anthropi; L-threonine deaminase from Escherichia coli; pyridoxal 5'-phosphate T=37°C; pH=7.5; 24 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Malik, M. Shaheer; Park, Eul-Soo; Shin, Jong-Shik
Green Chemistry, 2012 , vol. 14, # 8 p. 2137 - 2140
44855-57-4
+
72-19-5
L-苏氨酸
→
反应条件
34566-04-6
(S)-2-氨基辛烷
+
693-16-3
(±)-4-氨基辛烷
+
1492-24-6
L-2-氨基丁酸
+
111-13-7
反应条件
(S)-selective ω-transaminase from Ochrobactrum anthropi; L-threonine deaminase from Escherichia coli; pyridoxal 5'-phosphate T=37°C; pH=7.5; 24 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Malik, M. Shaheer; Park, Eul-Soo; Shin, Jong-Shik
Green Chemistry, 2012 , vol. 14, # 8 p. 2137 - 2140
44855-57-4
→
反应条件
21663-52-5
反应条件
Behandlung des Reaktionsprodukts mit HgCl2;
参考文献
Jahn
Monatshefte fuer Chemie, 1882 , vol. 3, p. 172
Chemische Berichte, 1875 , vol. 8, p. 805
44855-57-4
→
反应条件
628-61-5
反应条件
N-chloro-succinimide; TolSO2Cl; O-(2,4-dinitro-phenyl)-hydroxylamine 3.) THF, hν, 16 h, room t.; Yield given. Multistep reaction;
参考文献
Collazo, Luis R.; Guziec, Frank S.; Hu, Wei-Xiao Jr.; Pankayatselvan, Ratnadevi
Tetrahedron Letters, 1994 , vol. 35, # 43 p. 7911 - 7914
44855-57-4
+
72-19-5
L-苏氨酸
→
反应条件
693-16-3
(±)-4-氨基辛烷
+
1492-24-6
L-2-氨基丁酸
+
111-13-7
反应条件
(S)-selective ω-transaminase from Ochrobactrum anthropi; L-threonine deaminase from Escherichia coli; pyridoxal 5'-phosphate T=37°C; pH=7.5; 24 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Malik, M. Shaheer; Park, Eul-Soo; Shin, Jong-Shik
Green Chemistry, 2012 , vol. 14, # 8 p. 2137 - 2140
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