calcium carbonate in chloroform; water
T=20°C; 16 h;
参考文献
Goodyer, Claire L. M.; Chinje, Edwin C.; Jaffar, Mohammed; Stratford, Ian J.; Threadgill, Michael D.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 19 p. 4189 - 4206
1: 42 percent / SOCl2 / 96 h / 20 °C
2: 36 percent / H2 / Pd/C / methanol / 16 h / 20 °C
3: 51 percent / CaCO3 / H2O; CHCl3 / 16 h / 20 °C
View Scheme
参考文献
Goodyer, Claire L. M.; Chinje, Edwin C.; Jaffar, Mohammed; Stratford, Ian J.; Threadgill, Michael D.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 19 p. 4189 - 4206
1: 36 percent / H2 / Pd/C / methanol / 16 h / 20 °C
2: 51 percent / CaCO3 / H2O; CHCl3 / 16 h / 20 °C
View Scheme
参考文献
Goodyer, Claire L. M.; Chinje, Edwin C.; Jaffar, Mohammed; Stratford, Ian J.; Threadgill, Michael D.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 19 p. 4189 - 4206
potassium carbonate in dichloromethane; water
13 h;
参考文献
Kyne, Graham M.; Light, Mark E.; Hursthouse, Mike B.; De Mendoza, Javier; Kilburn, Jeremy D.
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 11 p. 1258 - 1263
