反应条件
1.1: 90 percent / NaBH4; CeCl3 / tetrahydrofuran; ethanol / 3 h / 20 °C 2.1: 90 percent / Jones' reagent / acetone / 5 h / 0 - 20 °C 3.1: (COCl)2 / 1,2-dichloro-ethane; dimethylformamide / 3 h / 20 °C 4.1: N-hydroxypyridine-2-thione; Et3N / tetrahydrofuran / 2 h / 20 °C 4.2: 83 mg / Bu3SnH / tetrahydrofuran / 4 h / 20 °C / Irradiation View Scheme
参考文献
Avenoza, Alberto; Barriobero, Jose I.; Busto, Jesus H.; Cativiela, Carlos; Peregrina, Jesus M.
Tetrahedron Asymmetry, 2002 , vol. 13, # 6 p. 625 - 632
