2-甲基异喹啉-1,3(2H,4H)-二酮合成路线 (共 17 条)
参考文献
Chemische Berichte, , vol. 21, p. 2299
反应条件
sodium ethanolate; copper in ethanol 3 h; Heating;
参考文献
Lowe, John A.; Newman, Michael E.
Synthetic Communications, 1987 , vol. 17, # 7 p. 803 - 808
反应条件
di-tert-butyl peroxide in 1,2-dichloro-benzene
Heating;
参考文献
Quiclet-Sire, Beatrice; Zard, Samir Z.
Chemical Communications, 2002 , # 20 p. 2306 - 2307
反应条件
in tetrahydrofuran; N,N-dimethyl-formamide
参考文献
American Home Products
Patent: US4927831 A1, 1990 ;
US 4927831 A
反应条件
triethylamine; acetone
T=20°C; P=1050.11 Torr; 3 h;
参考文献
Vicente, Jose; Gonzalez-Herrero, Pablo; Frutos-Pedreno, Roberto; Chicote, Maria-Teresa; Jones, Peter G.; Bautista, Delia
Organometallics, 2011 , vol. 30, # 5 p. 1079 - 1093
反应条件
T=180°C; Substitution;
参考文献
Ling, Ke-Qing; Ye, Jia-Hai; Chen, Xian-Yang; Ma, De-Jian; Xu, Jian-Hua
Tetrahedron, 1999 , vol. 55, # 30 p. 9185 - 9204
反应条件
in water
8 h; Ambient temperature;
参考文献
Wolfbeis, Otto S.; Trummer, Iris; Knierzinger, Andreas
Liebigs Annalen der Chemie, 1981 , # 5 p. 811 - 818
反应条件
1: toluene / Heating
2: acetonitrile
3: 56 percent / t-BuOO(Bu-t) / 1,2-dichloro-benzene / Heating
View Scheme
参考文献
Quiclet-Sire, Beatrice; Zard, Samir Z.
Chemical Communications, 2002 , # 20 p. 2306 - 2307
反应条件
1: 0.75 g / HCl-gas / 1.) 4h, room temperature, 2.) 2h, reflux
2: 0.24 g / H2O / 3 h / Heating
View Scheme
参考文献
Datta, D.; Tirodkar, R. B.; Usgaonkar, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 8 p. 641 - 643
反应条件
diethylamine in methanol; chloroform; benzene
1.) 50 deg C, 1 h; 2.) RT, overnight;
参考文献
Fujimaki; Nagase; Yamaguchi; et al.
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 7 p. 2663 - 2670