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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
450-16-8
合成路线
（共 11 条）
117285-87-7
→
反应条件
450-16-8
反应条件
dodec-1-ene; palladium on activated charcoal in diphenylether Heating;
参考文献
Cairns, Nicholas; Harwood, Laurence M.; Astles, David P.
Tetrahedron Letters, 1988 , vol. 29, # 11 p. 1311 - 1314
117285-75-3
→
反应条件
450-16-8
反应条件
palladium on activated charcoal in diphenylether 3 h; Heating;
参考文献
Cairns, Nicholas; Harwood, Laurence M.; Astles, David P.
Tetrahedron, 1992 , vol. 48, # 36 p. 7581 - 7590
531-59-9
7-甲氧基香豆素
→
反应条件
450-16-8
反应条件
1: 92 percent / methanol / 5 h / Heating 2: 100 percent / H2 / 5percent Pd/C / ethyl acetate / 1 h / 760 Torr / Ambient temperature 3: 96 percent / benzene / 5 h / Heating 4: 65 percent / AlCl3 / nitromethane / 0.5 h / Ambient temperature; other substrates 5: 66 percent / 5percent Pd/C / diphenyl ether / 3 h / Heating View Scheme
参考文献
Cairns, Nicholas; Harwood, Laurence M.; Astles, David P.
Tetrahedron, 1992 , vol. 48, # 36 p. 7581 - 7590
93198-68-6
→
反应条件
450-16-8
反应条件
1: 100 percent / H2 / 5percent Pd/C / ethyl acetate / 1 h / 760 Torr / Ambient temperature 2: 96 percent / benzene / 5 h / Heating 3: 65 percent / AlCl3 / nitromethane / 0.5 h / Ambient temperature; other substrates 4: 66 percent / 5percent Pd/C / diphenyl ether / 3 h / Heating View Scheme
参考文献
Cairns, Nicholas; Harwood, Laurence M.; Astles, David P.
Tetrahedron, 1992 , vol. 48, # 36 p. 7581 - 7590
117285-69-5
→
反应条件
450-16-8
反应条件
1: 65 percent / AlCl3 / nitromethane / 0.5 h / Ambient temperature; other substrates 2: 66 percent / 5percent Pd/C / diphenyl ether / 3 h / Heating View Scheme
参考文献
Cairns, Nicholas; Harwood, Laurence M.; Astles, David P.
Tetrahedron, 1992 , vol. 48, # 36 p. 7581 - 7590
69471-28-9
→
反应条件
450-16-8
反应条件
1: 96 percent / benzene / 5 h / Heating 2: 65 percent / AlCl3 / nitromethane / 0.5 h / Ambient temperature; other substrates 3: 66 percent / 5percent Pd/C / diphenyl ether / 3 h / Heating View Scheme
参考文献
Cairns, Nicholas; Harwood, Laurence M.; Astles, David P.
Tetrahedron, 1992 , vol. 48, # 36 p. 7581 - 7590
144582-47-8
→
反应条件
450-16-8
反应条件
1: Lewis acid 2: H2 / Pd/C 3: 95 percent / pyridine / Ambient temperature 4: 73 percent / AlCl3 / nitromethane / 0.5 h / from 0 deg C to r.t. 5: 40 percent / Pd/C / diphenyl ether / Heating View Scheme
参考文献
Cairns, Nicholas; Harwood, Laurence M.; Astles, David P.
Tetrahedron Letters, 1988 , vol. 29, # 11 p. 1311 - 1314
117285-78-6
→
反应条件
450-16-8
反应条件
1: 96 percent / H2 / Pd/C 2: 65 percent / AlCl3 / nitromethane / 0.5 h / from 0 deg C to r.t. 3: 90 percent / diphenyl ether / Heating 4: 66 percent / 1-dodecene / Pd/C / diphenyl ether / Heating View Scheme
参考文献
Cairns, Nicholas; Harwood, Laurence M.; Astles, David P.
Tetrahedron Letters, 1988 , vol. 29, # 11 p. 1311 - 1314
117285-76-4
→
反应条件
450-16-8
反应条件
palladium on activated charcoal in diphenylether Heating;
参考文献
Cairns, Nicholas; Harwood, Laurence M.; Astles, David P.
Tetrahedron Letters, 1988 , vol. 29, # 11 p. 1311 - 1314
117285-70-8
→
反应条件
450-16-8
反应条件
1: 73 percent / AlCl3 / nitromethane / 0.5 h / from 0 deg C to r.t. 2: 40 percent / Pd/C / diphenyl ether / Heating View Scheme
参考文献
Cairns, Nicholas; Harwood, Laurence M.; Astles, David P.
Tetrahedron Letters, 1988 , vol. 29, # 11 p. 1311 - 1314
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