in tetrahydrofuran
dilute (0.03 M) solns. of reagents were added simultaneously to THF over 2 h at 25°C; purified by reverse phase chromy. and recrystn.;
参考文献
Newcomb, Martin; Blanda, Michael T.; Azuma, Yutaka; Delord, Terry J.
Journal of the Chemical Society, Chemical Communications, 1984 , # 17 p. 1159 - 1160
Newcomb, Martin; Blanda, Michael T.; Azuma, Yutaka; Delord, Terry J.
Journal of the Chemical Society, Chemical Communications, 1984 , # 17 p. 1159 - 1160
in tetrahydrofuran
0.03 M solns. of reagents adding over 2 h to THF at 25 degree.C; purified by preparative reverse phase chromy. and recrystn. from MeOH-THF, identified by X-ray crystallography, NMR spectra, and elem. anal.;
参考文献
Newcomb, Martin; Blanda, Michael T.; Azuma, Yutaka; Delord, Terry J.
Journal of the Chemical Society, Chemical Communications, 1984 , # 17 p. 1159 - 1160
Newcomb, Martin; Blanda, Michael T.; Azuma, Yutaka; Delord, Terry J.
Journal of the Chemical Society, Chemical Communications, 1984 , # 17 p. 1159 - 1160