1,2,4,5-苯四胺 四盐酸盐合成路线 （共 6 条）
反应条件
1: With tin; Degussa F101 catalyst; hydrogen in ethanol T=80.5°C; P=15514.9 Torr; 2 h; AutoclaveInert atmosphere; 2: With hydrogenchloride in ethanol; water T=15°C;
参考文献
E I DU PONT DE NEMOURS AND COMPANY; GOLDFINGER, MARC B.; PELLENBARG, TIMOTHY
Patent: US2014/66629 A1, 2014 ;
Location in patent: Paragraph 0073-0075 ;
反应条件
sodium cyanoborohydride in water; acetonitrile
参考文献
Staab, Heinz A.; Elbl-Weiser, Karin; Krieger, Claus
European Journal of Organic Chemistry, 2000 , # 2 p. 327 - 333
反应条件
sodium acetate in ethanol; water 0.5 h; Heating;
参考文献
Kobayashi, Tomoshige; Kobayashi, Sayuri
European Journal of Organic Chemistry, 2002 , # 13 p. 2066 - 2073
反应条件
water; sodium hydrogencarbonate
参考文献
Harley-Mason; Laird
Tetrahedron, 1959 , vol. 7, p. 70,76
反应条件
triethylamine in tetrahydrofuran
参考文献
Siri, Olivier; Braunstein, Pierre; Rohmer, Marie-Madeleine; Benard, Marc; Welter, Richard
Journal of the American Chemical Society, 2003 , vol. 125, # 45 p. 13793 - 13803
反应条件
1: 48 percent / TEA / toluene / 0.33 h / Ambient temperature
2: 0.33 h / 400 °C
View Scheme
参考文献
Mataka, Shuntaro; Irie, Takashi; Ikezaki, Youji; Tashiro, Masashi
Chemische Berichte, 1993 , vol. 126, # 8 p. 1819 - 1822
