2-乙酰氨基-2-脱氧-3,4,6-三-邻乙酰基-beta-d-吡喃葡萄糖胺合成路线 （共 17 条）
反应条件
hydrogen; palladium on activated charcoal in methanol 0.5 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 36, # 21 p. 3635 - 3638
反应条件
1: NaN3; nBu4NHSO4; aq. NaHCO3 / CH2Cl2 / 2 h / 20 °C 2: H2; Et3N / Pd/C / ethyl acetate / 0.5 h View Scheme
参考文献
Organic Letters, , vol. 8, # 22 p. 5009 - 5012
反应条件
tetrakis(triphenylphosphine) palladium(0); diethylamine in tetrahydrofuran T=30°C; 0.333333 h;
参考文献
Chemical Communications, , # 47 p. 4952 - 4954
反应条件
palladium monocarbide in methanol
反应条件
piperidine in tetrahydrofuran
参考文献
Tetrahedron Letters, , vol. 31, # 48 p. 6987 - 6990
反应条件
1: 69 percent / iodine / acetonitrile / 14 h / 0 °C 2: 84 percent / DMAP / pyridine / 24 h / 20 °C 3: 79 percent / DMAP; Et3N / CH2Cl2 / 30 °C 4: 90 percent / samarium; CH2I2 / tetrahydrofuran; H2O / 1 h / 20 °C 5: (Ph3P)4Pd; Et2NH / tetrahydrofuran / 0.33 h / 30 °C View Scheme
参考文献
Chemical Communications, , # 47 p. 4952 - 4954
反应条件
piperidine in tetrahydrofuran 0.166667 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 13 p. 1461 - 1472
反应条件
3 A molecular sieve; bis(tri-n-butyltin)oxide in benzene T=20°C; 16 h;
参考文献
European Journal of Organic Chemistry, , # 2 p. 383 - 390
反应条件
1: 84 percent / DMAP / pyridine / 24 h / 20 °C 2: 79 percent / DMAP; Et3N / CH2Cl2 / 30 °C 3: 90 percent / samarium; CH2I2 / tetrahydrofuran; H2O / 1 h / 20 °C 4: (Ph3P)4Pd; Et2NH / tetrahydrofuran / 0.33 h / 30 °C View Scheme
参考文献
Chemical Communications, , # 47 p. 4952 - 4954
反应条件
1: 79 percent / DMAP; Et3N / CH2Cl2 / 30 °C 2: 90 percent / samarium; CH2I2 / tetrahydrofuran; H2O / 1 h / 20 °C 3: (Ph3P)4Pd; Et2NH / tetrahydrofuran / 0.33 h / 30 °C View Scheme
参考文献
Chemical Communications, , # 47 p. 4952 - 4954
