(1S,2S)-(-)-1-苯基亚丙基环氧合成路线 （共 41 条）
反应条件
potassium peroxymonosulfate; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; Shi epoxidation catalist in DMM; water; acetonitrile T=-10°C; 2 h; Na2B4O7; Na2EDTA buffer;
参考文献
Shi, Yian
Patent: US6348608 B1, 2002 ;
Location in patent: Page column 27 ;
反应条件
potassium carbonate; tetra(n-butyl)ammonium hydrogen sulphate; triethylamine in aq. Na2EDTA; water; acetonitrile; pentane
参考文献
Colorado State University Research Foundation
Patent: US2002/133031 A1, 2002 ;
Title/Abstract Full Text Show Details
Colorado State University Research Foundation
Patent: US6686483 B2, 2004 ;
反应条件
potassium carbonate; tetra(n-butyl)ammonium hydrogen sulphate in water; (ethylenedinitrilo)tetraacetic acid disodium salt; acetonitrile
参考文献
Colorado State University Research Foundation
Patent: US2002/133031 A1, 2002 ;
Title/Abstract Full Text Show Details
Colorado State University Research Foundation
Patent: US6686483 B2, 2004 ;
反应条件
(R,R)-(salen)Cr(III)-Cl in dichloromethane T=0°C; 48 h;
参考文献
Kureshy, Rukhsana Ilays; Prathap, K. Jeya; Kumar, Manish; Bera, Prasanta Kumar; Khan, Noor-Ul Hasan; Abdi, Sayed Hasan Razi; Bajaj, Hari Chandra
Tetrahedron, 2011 , vol. 67, # 43 p. 8300 - 8307
反应条件
pyridine 1-oxide; C46H48ClMnN2O4; C92H96Cl2Mn2N4O8; urea hydrogen peroxide addition compound in methanol T=5 - 20°C; 6 h; enantioselective reaction;
参考文献
Maity, Nabin Ch.; Rao, Ganga V.S.; Prathap; Abdi, Sayed H.R.; Kureshy, Rukhsana I.; Khan, Noor-Ul H.; Bajaj, Hari C.
Journal of Molecular Catalysis A: Chemical, 2013 , vol. 366, p. 380 - 389
反应条件
C60H42Cl5N2O3Ru; oxygen in chlorobenzene T=25°C; 24 h; optical yield given as percent eeenantioselective reaction;
参考文献
Koya, Shota; Nishioka, Yota; Mizoguchi, Hirotaka; Uchida, Tatsuya; Katsuki, Tsutomu
Angewandte Chemie - International Edition, 2012 , vol. 51, # 33 p. 8243 - 8246
反应条件
chiral polymer-based chromium salen in dichloromethane T=-10°C; 36 h; Title compound not separated from byproducts;
参考文献
Kureshy, Rukhsana Ilays; Prathap, K. Jeya; Kumar, Manish; Bera, Prasanta Kumar; Khan, Noor-Ul Hasan; Abdi, Sayed Hasan Razi; Bajaj, Hari Chandra
Tetrahedron, 2011 , vol. 67, # 43 p. 8300 - 8307
反应条件
C68H92Cr2N8O4(2+)*2Cl(1-) in methanol; dichloromethane T=20°C; 30 h; optical yield given as percent eeenantioselective reaction;
参考文献
Kureshy, Rukhsana Ilays; Prathap, K. Jeya; Kumar, Manish; Bera, Prasanta Kumar; Khan, Noor-Ul Hasan; Abdi, Sayed Hasan Razi; Bajaj, Hari Chandra
Tetrahedron, 2011 , vol. 67, # 43 p. 8300 - 8307
反应条件
C68H92Cr2N8O4(2+)*2Cl(1-) in methanol; dichloromethane T=20°C; 20 h; optical yield given as percent eeenantioselective reaction;
参考文献
Kureshy, Rukhsana Ilays; Prathap, K. Jeya; Kumar, Manish; Bera, Prasanta Kumar; Khan, Noor-Ul Hasan; Abdi, Sayed Hasan Razi; Bajaj, Hari Chandra
Tetrahedron, 2011 , vol. 67, # 43 p. 8300 - 8307
反应条件
C68H92Cr2N8O4(2+)*2Cl(1-) in methanol; dichloromethane T=20°C; 24 h; optical yield given as percent eeenantioselective reaction;
参考文献
Kureshy, Rukhsana Ilays; Prathap, K. Jeya; Kumar, Manish; Bera, Prasanta Kumar; Khan, Noor-Ul Hasan; Abdi, Sayed Hasan Razi; Bajaj, Hari Chandra
Tetrahedron, 2011 , vol. 67, # 43 p. 8300 - 8307
