反应条件
1: 1.) 6 M sulfuric acid, NaNO2, 2.) CuSO4*5H2O, 96percent H2SO4 / 1.) water, 2.) 165 deg C 2: 84 percent / K2CO3 / acetone / 5 h / Heating 3: 70 percent / potassium permanganate, pyridine / H2O / 1.) 50 deg C, 3 h, 2.) RT, 3 h 4: 95 percent / LiAlH4 / diethyl ether / 3 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 33, # 9 p. 2408 - 2412
