3,4,5-三甲氧基苯甲酰氯合成路线 （共 203 条）
反应条件
1: pyridine / 1) 0-5 deg C 2) 1h, room temperature
2: 85 percent / pyridine; H2O / 10 h / Heating
3: SOCl2 / benzene / 6 h / Heating
4: 75 percent / benzene / 2 h / Heating
View Scheme
参考文献
Husain, M. I.; Srivastava, G. C.; Dua, P. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 381 - 383
反应条件
1: pyridine / 1) 0-5 deg C 2) 1h, room temperature
2: 75 percent / pyridine; H2O / 10 h / Heating
3: SOCl2 / benzene / 6 h / Heating
4: 64 percent / benzene / 2 h / Heating
View Scheme
参考文献
Husain, M. I.; Srivastava, G. C.; Dua, P. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 381 - 383
反应条件
1: pyridine / 1) 0-5 deg C 2) 1h, room temperature
2: 75 percent / pyridine; H2O / 10 h / Heating
3: SOCl2 / benzene / 6 h / Heating
4: 72 percent / benzene / 2 h / Heating
View Scheme
参考文献
Husain, M. I.; Srivastava, G. C.; Dua, P. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 381 - 383
反应条件
1: pyridine / 1) 0-5 deg C 2) 1h, room temperature
2: 72 percent / pyridine; H2O / 10 h / Heating
3: SOCl2 / benzene / 6 h / Heating
4: 71 percent / benzene / 2 h / Heating
View Scheme
参考文献
Husain, M. I.; Srivastava, G. C.; Dua, P. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 381 - 383
反应条件
1: pyridine / 1) 0-5 deg C 2) 1h, room temperature
2: 85 percent / pyridine; H2O / 10 h / Heating
3: SOCl2 / benzene / 6 h / Heating
4: 75 percent / benzene / 2 h / Heating
View Scheme
参考文献
Husain, M. I.; Srivastava, G. C.; Dua, P. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 381 - 383
反应条件
1: pyridine / 1) 0-5 deg C 2) 1h, room temperature
2: 25 percent / pyridine; H2O / 10 h / Heating
3: SOCl2 / benzene / 6 h / Heating
4: 70 percent / benzene / 2 h / Heating
View Scheme
参考文献
Husain, M. I.; Srivastava, G. C.; Dua, P. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 381 - 383
反应条件
sodium hydroxide
0.25 h;
参考文献
Kar
Pharmazie, 1983 , vol. 38, # 5 p. 313 - 315
反应条件
potassium thioacyanate in acetonitrile
T=20°C; 0.25 h;
参考文献
Poitout, Lydie; Brault, Valerie; Ferrandis, Eric; Thurieau, Christophe
Patent: US2005/49290 A1, 2005 ;
Location in patent: Page/Page column 33 ;
US 20050049290 A1
参考文献
Smith,P.A.S.; Emerson,D.W.
Journal of the American Chemical Society, 1960 , vol. 82, p. 3076 - 3082
Full Text View citing articles Show Details
deStevens,G. et al.
Journal of Organic Chemistry, 1964 , vol. 29, p. 1115 - 1119
反应条件
in acetone
T=20°C; Reflux;
参考文献
Saeed, Aamer; Al-Masoudi, Najim A.; Ahmed, Amjed A.; Pannecouque, Christophe
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2011 , vol. 66, # 5 p. 512 - 520
