3,4,5-三甲氧基苯甲酰氯合成路线 （共 203 条）
反应条件
1: 3.02 g / N-ethyl-N,N-diisopropylamine / CH2Cl2
2: 71 percent / hydrazine hydrate / ethanol / 24 h / Heating
View Scheme
参考文献
Elsinghorst, Paul W.; Gonzalez Tanarro, Camino M.; Guetschow, Michael
Journal of Medicinal Chemistry, 2006 , vol. 49, # 25 p. 7540 - 7544
反应条件
1: 2.20 g / N-ethyl-N,N-diisopropylamine / CH2Cl2
2: 80 percent / hydrazine hydrate / ethanol / 24 h / Heating
View Scheme
参考文献
Elsinghorst, Paul W.; Gonzalez Tanarro, Camino M.; Guetschow, Michael
Journal of Medicinal Chemistry, 2006 , vol. 49, # 25 p. 7540 - 7544
反应条件
1: 2.91 g / N-ethyl-N,N-diisopropylamine / CH2Cl2
2: 66 percent / hydrazine hydrate / ethanol / 24 h / Heating
View Scheme
参考文献
Elsinghorst, Paul W.; Gonzalez Tanarro, Camino M.; Guetschow, Michael
Journal of Medicinal Chemistry, 2006 , vol. 49, # 25 p. 7540 - 7544
反应条件
1: 3.05 g / N-ethyl-N,N-diisopropylamine / CH2Cl2
2: 65 percent / hydrazine hydrate / ethanol / 24 h / Heating
View Scheme
参考文献
Elsinghorst, Paul W.; Gonzalez Tanarro, Camino M.; Guetschow, Michael
Journal of Medicinal Chemistry, 2006 , vol. 49, # 25 p. 7540 - 7544
反应条件
1: 3.24 g / N-ethyl-N,N-diisopropylamine / CH2Cl2 / 1 h
2: 77 percent / hydrazine hydrate / ethanol / 24 h / Heating
View Scheme
参考文献
Elsinghorst, Paul W.; Gonzalez Tanarro, Camino M.; Guetschow, Michael
Journal of Medicinal Chemistry, 2006 , vol. 49, # 25 p. 7540 - 7544
反应条件
Pd-BaSO4; xylene
Hydrogenation;
参考文献
Mauthner
Journal fuer Praktische Chemie (Leipzig), 1931 , vol. <2> 129, p. 278
Full Text Show Details
Frank; Fanta; Tarbell
Journal of the American Chemical Society, 1948 , vol. 70, p. 2314,2317
反应条件
Hydrogenation.Nebenprodukt;
参考文献
Spaeth
Monatshefte fuer Chemie, 1919 , vol. 40, p. 138
Monatshefte fuer Chemie, 1921 , vol. 42, p. 263
参考文献
Sharp
Journal of the Chemical Society, 1936 , p. 1234
Full Text Show Details
Frank; Fanta; Tarbell
Journal of the American Chemical Society, 1948 , vol. 70, p. 2314,2317
反应条件
1: aq. NaHCO3
2: N2H4*H2O
View Scheme
参考文献
Roehnert,H.
Archiv der Pharmazie und Berichte der Deutschen Pharmazeutischen Gesellschaft, 1962 , vol. 295, p. 697 - 706
反应条件
in ethanol; chloroform; benzene
36 h; Ambient temperature;
参考文献
Bartl; Svatek; Dlabac; et al.
Collection of Czechoslovak Chemical Communications, 1984 , vol. 49, # 8 p. 1816 - 1826
