3,4,5-三甲氧基苯甲酰氯合成路线 （共 203 条）
反应条件
N-methylamine hydrochloride; N-ethyl-N,N-diisopropylamine in tetrahydrofuran; ethyl acetate
参考文献
Sonn; Meyer
Chemische Berichte, 1925 , vol. 58, p. 1102
参考文献
Vekemans, Jozef; Hoornaert, Georges
Tetrahedron, 1980 , vol. 36, p. 943 - 950
反应条件
triethylamine in dichloromethane
T=0°C;
参考文献
Kong, Wangqing; Casimiro, Maria; Fuentes, Noelia; Merino, Estibaliz; Nevado, Cristina
Angewandte Chemie - International Edition, 2013 , vol. 52, # 49 p. 13086 - 13090
Angew. Chem., 2013 , vol. 125, # 49 p. 13324 - 13328,5
反应条件
1: With N,N,N',N,-tetramethylethylenediamine in diethyl ether
T=0 - 20°C; Cooling with ice;
2: With hydrogenchloride; water in diethyl ether
参考文献
TRANSITIONS OPTICAL, INC.
Patent: WO2012/82999 A1, 2012 ;
Location in patent: Page/Page column 52 ;
反应条件
hydrogenchloride in tetrahydrofuran; diethyl ether; hexane
参考文献
TRANSITIONS OPTICAL, INC.
Patent: US2012/156508 A1, 2012 ;
反应条件
diethyl ether; benzene
参考文献
Moffett,R.B. et al.
Journal of Medicinal Chemistry, 1964 , vol. 7, p. 178 - 186
Full Text View citing articles Show Details
Koelsch; Flesch
Journal of Organic Chemistry, 1955 , vol. 20, p. 1270,1273
反应条件
(i) CdCl2, (ii) /BRN= 403117/; Multistep reaction;
参考文献
Moffett,R.B. et al.
Journal of Medicinal Chemistry, 1964 , vol. 7, p. 178 - 186
反应条件
triethylamine in dichloromethane
参考文献
Gita, Haruhisa; Sobe, Yoshiaki; Akaku, Haruo; Ekine, Rena; Oto, Yuso; Isawa, Satoru; Hayashi, Hideya
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 4 p. 549 - 551
参考文献
CIBA
Patent: DE608412 , 1932 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 20, p. 763
参考文献
Perun,T.J. et al.
Journal of Organic Chemistry, 1963 , vol. 28, # 11 p. 2937 - 2943
